PROPERTIES OF THE KETO AMIDES FORMED BY AMINOLYSIS OF 3,7-DIARYLPYRANO[4,3-c]PYRAN-l,5-DIONE DERIVATIVES:A SOLID-STATE REACTION,CRYSTAL STRUCTURES,AND THERMAL ANALYSIS

Chika Kawabe; Keitaro Kawakita; Masanori Morinaga

首页> 外文期刊>Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry >PROPERTIES OF THE KETO AMIDES FORMED BY AMINOLYSIS OF 3,7-DIARYLPYRANO[4,3-c]PYRAN-l,5-DIONE DERIVATIVES:A SOLID-STATE REACTION,CRYSTAL STRUCTURES,AND THERMAL ANALYSIS

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PROPERTIES OF THE KETO AMIDES FORMED BY AMINOLYSIS OF 3,7-DIARYLPYRANO[4,3-c]PYRAN-l,5-DIONE DERIVATIVES:A SOLID-STATE REACTION,CRYSTAL STRUCTURES,AND THERMAL ANALYSIS

机译：通过3,7-二芳基吡喃并[4,3-c]吡喃-1,5-二酮衍生物的胺化反应制得的酮基酰胺：固相反应，晶体结构和热分析

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Aminolysis of 3,7-diarylpyrano[4,3-c]pyran-l,5-dione derivatives gave keto amides,which upon heating returned back to the original compounds in the solid state.X-Ray crystallographic analysis of the keto amides showed proximate orientations of the ketone and the amide groups.TGA and DTA of the keto amides clarified a kind of solid-state reaction which occurred in appearance without melting,but microscopically proceeded via melting of the keto amides,structural change,and crystallization of the products.

机译：对3,7-二芳基吡喃并[4,3-c]吡喃-1,5-二酮衍生物进行氨解反应，得到酮酰胺，加热后又回到固态，回到原来的化合物。X-射线晶体学分析酮酰胺酮酰胺的TGA和DTA澄清了一种固态反应，该反应在外观上没有熔化，但在微观上通过酮酰胺的熔化，结构变化和产物结晶而进行。。

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《Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry》 |2007年第9期|共11页
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Chika Kawabe; Keitaro Kawakita; Masanori Morinaga;
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1. PROPERTIES OF THE KETO AMIDES FORMED BY AMINOLYSIS OF 3,7-DIARYLPYRANO[4,3-c]PYRAN-l,5-DIONE DERIVATIVES:A SOLID-STATE REACTION,CRYSTAL STRUCTURES,AND THERMAL ANALYSIS [J] . Chika Kawabe, Keitaro Kawakita, Masanori Morinaga Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry . 2007,第9期

机译：通过3,7-二芳基吡喃并[4,3-c]吡喃-1,5-二酮衍生物的胺化反应制得的酮基酰胺：固相反应，晶体结构和热分析
2. Creation of Concave-Shaped Conformation in Crystal Structures Using an Iminodicarbonyl Linker.An Application to Solid-State Intramolecular [4 + 4] Photocycloaddition Reactions of 2-Pyridone Derivatives [J] . Hyuma Masu, Ken Ohmori, Keiki Kishikawa, Bulletin of the Chemical Society of Japan . 2005,第6期

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机译：晶体化学的边界：结构和性质的预测。第2部分。水晶结构预测的固态性质和反应。晶体中晶体晶状态反应的观察及晶体不稳定反应中间体的结构。

PROPERTIES OF THE KETO AMIDES FORMED BY AMINOLYSIS OF 3,7-DIARYLPYRANO[4,3-c]PYRAN-l,5-DIONE DERIVATIVES:A SOLID-STATE REACTION,CRYSTAL STRUCTURES,AND THERMAL ANALYSIS

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