Syntheses and properties of new poly(amide-imide)s based on 1,4-bis(4-aminophenoxy)naphthalene and various diimide-diacids

Chen JA.; Yang CP.

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Syntheses and properties of new poly(amide-imide)s based on 1,4-bis(4-aminophenoxy)naphthalene and various diimide-diacids

机译：基于1,4-双（4-氨基苯氧基）萘和各种二酰亚胺-二酸的新型聚（酰胺-酰亚胺）的合成与性能

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A series of new alternative poly(amide-imide)s (PAIs, IIIa-j) was synthesized by the direct polycondensation of 1,4-bis(4-aminophenoxy)naphthalene (1,4-BAPON) with various aromatic diimide-diacids. These polymers were obtained in quantitative yields with inherent viscosities of 0.71-1.03 dL/g. Except for IIIa, most of the polymers were soluble in aprotic polar solvents such as NMP, DMAc, DMF, and DMSO and could be solution-cast into transparent, flexible, and tough films. The glass transition temperatures of these PAIs were in the range of 235-280 degrees C. Thermogravimetric analyses established that these polymers were fairly stable up to 450 degrees C, and 10% weight; loss temperatures were recorded in the range of 520-569 degrees C under nitrogen and 506-566 degrees C under an air atmosphere, Compared with the PAIs with the 1,4-bis(4-aminophenoxy)benzene structure (series TV), the solubility of series III was better than that of series TV. Series III also exhibited lower crystallinity and better processability than those of series TV. (C) 2000 John Wiley & Sons, Inc. [References: 21]

机译：通过将1,4-双（4-氨基苯氧基）萘（1,4-BAPON）与各种芳族二酰亚胺-二酸直接缩聚合成了一系列新的替代聚（酰胺-酰亚胺）（PAI，IIIa-j）。这些聚合物以定量收率获得，固有粘度为0.71-1.03 dL / g。除IIIa外，大多数聚合物可溶于非质子极性溶剂（如NMP，DMAc，DMF和DMSO）中，并可溶液浇铸成透明，柔性和坚韧的薄膜。这些PAI的玻璃化转变温度在235-280℃的范围内。热重分析确定这些聚合物在最高450℃和10％重量的条件下是相当稳定的。损失温度在氮气下记录为520-569℃，在大气中记录为506-566℃。与具有1,4-双（4-氨基苯氧基）苯结构的PAI相比，TV系列III系列的溶解度优于TV系列。 III系列还显示出比系列TV更低的结晶度和更好的可加工性。（C）2000 John Wiley＆Sons，Inc. [参考：21]

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《Journal of Applied Polymer Science》 |2000年第1期|共9页
作者
Chen JA.; Yang CP.;
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正文语种 eng
中图分类高分子化学（高聚物）;高分子化合物产品;有机化学;
关键词
1; 4-bis(4-aminophenoxy)naphthalene; Aromatic poly(amide-imide); Direct polycondensation; Aromatic tetracarboxylic dianhydrides; Direct polycondensation; Trimellitic anhydride; Triphenyl phosphite; Polyimides; Diamines;

机译：1;4-双（4-氨基苯氧基）萘;芳族聚（酰胺-酰亚胺）;直接缩聚;芳族四羧酸二酐;直接缩聚;三苯四酸酐;亚磷酸三苯酯;聚酰亚胺;二胺;

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1. Syntheses and properties of new poly(amide-imide)s based on 1,4-bis(4-aminophenoxy)naphthalene and various diimide-diacids [J] . Chen JA., Yang CP. Journal of Applied Polymer Science . 2000,第1期

机译：基于1,4-双（4-氨基苯氧基）萘和各种二酰亚胺-二酸的新型聚（酰胺-酰亚胺）的合成与性能
2. Synthesis and properties of poly(amide-imide)s based on the diimide-diacid condensed from 2,2 ' bis(4-aminophenoxy)biphenyl and trimellitic anhydride [J] . Yang CP., Liou GS., Jeng SH. Journal of Polymer Science, Part A. Polymer Chemistry . 1998,第7期

机译：由2,2'双（4-氨基苯氧基）联苯和偏苯三酸酐缩合的二酰亚胺-二酸聚（酰胺-酰亚胺）的合成与性能
3. New poly(amide-imide)s syntheses, 16 Preparation and properties of poly(amide-imide)s derived from 3,3-bis[4-(4-aminophenoxy)phenyl]phthalide and various bis(trimellitimide)s [J] . Cnin-Ping Yang, Jiun-Hung Lin Macromolecular chemistry and physics . 1995,第12期

机译：新的聚（酰胺-酰亚胺）s的合成，16衍生自3,3-双[4-（4-（4-氨基苯氧基）苯基]邻苯二甲酰亚胺和各种双（三苯甲酰亚胺）s的聚（酰胺-酰亚胺）s的制备和性能
4. Syntheses of biocompatible polyimide and poly(amide-imide) containing phosphorylcholine moiety and the coating ability of the nanosheets [C] . Mari Ogino, Kohei Asao, Haruki Oka, World biomaterials congress . 2016

机译：含磷酰胆碱部分的生物相容性聚酰亚胺和聚（酰胺-酰亚胺）的合成及其纳米片的包覆能力
5. I. Synthesis of substituted naphthalenes utilizing active nickel. II. Synthesis of substituted naphthoquinones and formation of a charge transfer complex. III. Synthesis of substituted 1,4-diphenyl-2-butenes from (eta(6):eta(6)-1,4-diphenyl-1,3-butadiene)-bis(tricarbonylchromium) [D] . Forkner, Matthew W. 1988

机译：I.利用活性镍合成取代的萘。二。取代萘醌的合成和电荷转移配合物的形成。三，由（eta（6）：eta（6）-1,4-二苯基-1,3-丁二烯）-双（三羰基铬）合成取代的1,4-二苯基-2-丁烯
6. Poly[aquabis(μ4-naphthalene-1,4-dicarboxylato)(1,10-phenanthroline-5,6-dione)dimanganese(II)] [O] . Fang-Di Cong, Feng-Yang Yu, Zhen Wei, 2016

机译：聚[aquabis（μ4-萘-1,4-二羧酸基）（1,10-菲咯啉-5,6-二酮）二锰（II）]
7. Synthesis and Properties of 1,4-Bis(4-aminophenoxy)naphthalene and Its Polyimides [O] . Chin-Ping Yang, Jhy-An Chen 1998

机译：1,4-双（4-氨基氧基氧基）萘及其聚酰亚胺的合成与性能
8. Epoxidation of E-1,4-poly(2-triethylsilyl-1,3-butadiene) and E-1,4-poly-(2,3-bis(trimethylsilyl)-1,3-butadiene). Stereochemical analysis of E-1,4-poly(2,3-epoxy-2-triethylsilyl-1,3-butadiene) and E-1,4-poly-(2,3-bis(trimethylsilyl [R] . Jiang, W., Weber, W. P. 1988

机译：E-1,4-聚（2-三乙基甲硅烷基-1,3-丁二烯）和E-1,4-聚 - （2,3-双（三甲基甲硅烷基）-1,3-丁二烯）的环氧化。 E-1,4-聚（2,3-环氧-2-甲基甲硅烷基-1,3-丁二烯）和E-1,4-聚 - （2,3-双（三甲基甲硅烷基）的立体化学分析

Syntheses and properties of new poly(amide-imide)s based on 1,4-bis(4-aminophenoxy)naphthalene and various diimide-diacids

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