Synthesis, Structure, and Characterization of Polymeric Stationary Phase Derived from (R,R)-Tartramide and Bisphenol-S

T. Jablonska-Plkus; W. Charmas; B. Podkoscielna; B. Gawdzik

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Synthesis, Structure, and Characterization of Polymeric Stationary Phase Derived from (R,R)-Tartramide and Bisphenol-S

机译：（R，R）-酒石酰胺和双酚-S衍生的聚合物固定相的合成，结构和表征

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The preparation of a new chiral polymeric stationary phase for chromatography is presented. A porous copolymer of mono- and dimethacrylate derivatives of bisphenol-S and divinylbenzene containing hydroxyl functional groups was used as a matrix. (3-Aminopropyl)triethoxysilane was used as a coupling agent and was bonded to these groups. The obtained compound was transferred into a final product during a three-step synthesis. The properties of the obtained polymeric phase with the chiral moiety were studied.

机译：介绍了一种用于色谱的新型手性聚合物固定相的制备。将双酚S的单和二甲基丙烯酸酯衍生物和含有羟基官能团的二乙烯基苯的多孔共聚物用作基质。使用（3-氨基丙基）三乙氧基硅烷作为偶联剂，并键合到这些基团上。在三步合成过程中，将获得的化合物转移到最终产物中。研究了获得的具有手性部分的聚合物相的性质。

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来源
《Journal of Applied Polymer Science》 |2001年第14期|共9页
作者
T. Jablonska-Plkus; W. Charmas; B. Podkoscielna; B. Gawdzik;
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正文语种 eng
中图分类高分子化学（高聚物）;高分子化合物产品;有机化学;
关键词
chiral porous copolymers; derivative of (R-R)-tartramide and bisphenol-S; chromagographic stationary phase;

机译：手性多孔共聚物;（R-R）-酒石酰胺和双酚-S的衍生物;色谱固定相;

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1. Synthesis, Structure, and Characterization of Polymeric Stationary Phase Derived from (R,R)-Tartramide and Bisphenol-S [J] . T. Jablonska-Plkus, W. Charmas, B. Podkoscielna, Journal of Applied Polymer Science . 2001,第14期

机译：（R，R）-酒石酰胺和双酚-S衍生的聚合物固定相的合成，结构和表征
2. Polymeric stationary phase, based on (R,R)-tartramide and bisphenol S, with potential chiral properties [J] . Jablonska-Pikus T, Charmas W, Podkoscielna B, Journal of Polymer Science, Part A. Polymer Chemistry . 2004,第10期

机译：基于（R，R）-酒石酰胺和双酚S的聚合物固定相，具有潜在的手性
3. Polymeric imidazolium ionic liquids as valuable stationary phases in gas chromatography: Chemical synthesis and full characterization [J] . Jaime Gonzalez-Alvarez, Domingo Blanco-Gomis, Pilar Arias-Abrodo Analytica chimica acta . 2012,第Null期

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Synthesis, Structure, and Characterization of Polymeric Stationary Phase Derived from (R,R)-Tartramide and Bisphenol-S

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