Microemulsion Polymerization of Methyl Methacrylate Initiated with #gamma# Ray

Xiangling Xu; Xuewu Ge; Zhicheng Zhang; Manwei Zhang; Ju Zuo; Aizhen Niu

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Microemulsion Polymerization of Methyl Methacrylate Initiated with #gamma# Ray

机译：＃gamma＃射线引发的甲基丙烯酸甲酯的微乳液聚合

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Polymerization of methyl methacrylate was studied in an oil and water microemulsion stabilized with styrene 12-butinoyloxy-9-octadecenoic acid. During the polymerization the size change of the monomer-swollen particles with conversion was measured with photon correlation spectroscopy, and the hydrodynamic, diameter of the final polymer latex was about 50 nm. The polymerization kinetics in this microemulsion were also investigated. The apparent plateau of the polymerization rate was observed at a low dose rate and high emulsifier content. The mechanism leading to this plateau was discussed.

机译：在用苯乙烯12-丁酰氧基-9-十八烯酸稳定的油水微乳液中研究了甲基丙烯酸甲酯的聚合。在聚合期间，通过光子相关光谱法测量单体溶胀颗粒随转化的尺寸变化，并且最终聚合物胶乳的流体动力学直径为约50nm。还研究了该微乳液中的聚合动力学。在低剂量率和高乳化剂含量下观察到聚合速率的表观平稳期。讨论了导致这种平台期的机制。

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《Journal of Applied Polymer Science》 |1999年第13期|共6页
作者
Xiangling Xu; Xuewu Ge; Zhicheng Zhang; Manwei Zhang; Ju Zuo; Aizhen Niu;
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正文语种 eng
中图分类高分子化学（高聚物）;高分子化合物产品;有机化学;
关键词
microemulsion polymerization; methyl methacrylate; polymerization kinetics;

机译：微乳液聚合甲基丙烯酸甲酯聚合动力学;

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专利

1. Microemulsion Polymerization of Methyl Methacrylate Initiated with #gamma# Ray [J] . Xiangling Xu, Xuewu Ge, Zhicheng Zhang, Journal of Applied Polymer Science . 1999,第13期

机译：＃gamma＃射线引发的甲基丙烯酸甲酯的微乳液聚合
2. Synthesis of Poly(methyl methacrylate) Nanoparticles Initiated by 2,2-Azoisobutyronitrile via Differential Microemulsion Polymerization [J] . Chaiwat Norakankorn, Qinmin Pan, Garry L. Rempel, Macromolecular rapid communications: Publishing the newsletters of the European Polymer Federation . 2007,第9期

机译：微细乳液聚合法合成2,2-偶氮异丁腈引发的聚甲基丙烯酸甲酯纳米粒子
3. Microemulsion polymerization of methyl methacrylate initiated with BPO [J] . Xiangling Xu, Xuewu Ge, Zhicheng Zhang, European Polymer Journal . 1999,第11期

机译：BPO引发的甲基丙烯酸甲酯的微乳液聚合
4. Graft Copolymerization of Methyl Methacrylate From Poly(Glycidyl Methacrylate-co-Styrene) Initiated by Cp2TiCl-Catalyzed Epoxide Radical Ring Opening [C] . Alexandru D. Asandei, Gobinda Saha PMSE Symposia . 2006

机译：CP2TICL催化环氧化物 - 开口引发的聚（甲基丙烯酸甲酯 - 共苯乙烯）从甲基丙烯酸甲酯的接枝共聚
5. Vibrational overtone spectroscopy of several mono- and polyacrylates, azo-initiators and polysiloxanes, vibrationally initiated polymerization of methyl methacrylate and methyl methacrylate-polysiloxane mixtures. [D] . Gerasimov, Timofey G. 2002

机译：几种单丙烯酸和聚丙烯酸酯，偶氮引发剂和聚硅氧烷的振动泛音谱，甲基丙烯酸甲酯和甲基丙烯酸甲酯-聚硅氧烷混合物的振动引发聚合。
6. A new initiating system based on (SiMes)Ru(PPh3)(Ind)Cl2 combined with azo-bis-isobutyronitrile in the polymerization and copolymerization of styrene and methyl methacrylate [O] . Abdullah M. Al-Majid, Waseem Sharaf Shamsan, Abdel-Basit Mohammed Al-Odayn, 2017

机译：SiMes Ru（PPh3）（Ind）Cl2与偶氮-双-异丁腈结合的新型引发体系用于苯乙烯和甲基丙烯酸甲酯的聚合和共聚
7. Microemulsion and Conventional Emulsion Co-polymerizations of p-Methyl Styrene with Methyl Methacrylate [O] . Ramana G. V. Reddy, Juby Thomas, P. K. Radhakrishnan 2008

机译：微乳液和常规乳液与甲基丙烯酸甲基甲基甲基苯乙烯的共聚物

Microemulsion Polymerization of Methyl Methacrylate Initiated with #gamma# Ray

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