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Characterization of the early Byzantine pottery from Cari?in Grad (South Serbia) in terms of composition and firing temperature

机译:从成分和烧成温度方面对Cari?in Grad(南塞尔维亚)的早期拜占庭陶器进行表征

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Mineralogical and chemical composition as well as production methods of the pottery from Cari?in Grad, a significant early Byzantine urban complex and production centre of the northern Illyricum region, were determined by multi-analytical investigations that comprised optical analysis and scanning electron microscopy with energy dispersive spectrometry (SEMeEDS), micro-Raman and Fourier transform infrared (FTIR) spectroscopy, and X-ray powder diffraction (XRPD) methods. The obtained data indicate that all investigated pottery samples were made of similar raw material that, most likely, originated from the local geological environment. Estimated firing temperatures for the cooking pots vary between 600 ℃ and 900 ℃, while for the glazed table and storage vessels they are more uniform, about 900 ℃. The transparent high lead glaze was obtained by direct application of lead oxide to the ceramic surface.
机译:通过包括光学分析和能量扫描电子显微镜在内的多分析研究确定了Cari?in Grad的矿物学和化学成分以及陶器的生产方法。分散光谱法(SEMeEDS),显微拉曼光谱和傅立叶变换红外光谱(FTIR)以及X射线粉末衍射(XRPD)方法。获得的数据表明,所有调查的陶器样品都是由相似的原材料制成的,这些原材料很可能起源于当地的地质环境。炊具的估计烧成温度在600℃至900℃之间变化,而釉面的桌子和储藏容器则更均匀,约为900℃。透明的高铅釉料是通过将氧化铅直接涂覆到陶瓷表面上而获得的。

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