Crystal structure of Ho_6Pb_9Se_(11) and magnetic properties of R_6Pb_2Se_(11) (R = Y, Dy and Ho)

L.D. Gulay; D. Kaczorowski; V.Ya. Shemet

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Crystal structure of Ho_6Pb_9Se_(11) and magnetic properties of R_6Pb_2Se_(11) (R = Y, Dy and Ho)

机译：Ho_6Pb_9Se_（11）的晶体结构和R_6Pb_2Se_（11）的磁性（R = Y，Dy和Ho）

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Single phase samples of .the R_6Pb_2Se_(11) (R = Y, Dy and Ho) compounds were obtained using high temperature synthesis. Crystal structure of Ho_6Pb_2Se_(11) (Y_6Pb_2Se_(11) type, space group Cmcm, Pearson symbol oC76, lattice parameters: a = 0.40603(7) nm, & = 1 .3397(3) nm, c = 3.7542(5) nm) was reinvestigated by means of X-ray single crystal diffraction and refined down to Rl = 0.0572. Magnetic properties of the R_6Pb_2Se_(11) compounds were studied in wide ranges of temperature and magnetic field. Dy_6Pb_2Se_(11) and Ho_6Pb_2Se_(11) were found to order antiferromagnetically at T_N = 2.2 and 2.4 K, respectively, whereas weak diamagnetism was established for Y_6Pb_2Se_(11).

机译：使用高温合成获得R_6Pb_2Se_（11）（R = Y，Dy和Ho）化合物的单相样品。 Ho_6Pb_2Se_（11）（Y_6Pb_2Se_（11）类型的晶体结构，Cmcm空间群，皮尔逊符号oC76，晶格参数：a = 0.40603（7）nm，＆= 1.3397（3）nm，c = 3.7542（5）nm借助X射线单晶衍射重新研究）并精制至R1 ＝ 0.0572。研究了R_6Pb_2Se_（11）化合物在较宽的温度和磁场范围内的磁性。发现Dy_6Pb_2Se_（11）和Ho_6Pb_2Se_（11）分别在T_N = 2.2和2.4 K时反铁磁有序，而Y_6Pb_2Se_（11）则建立了弱的反磁性。

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《Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics》 |2006年第2期|共4页
作者
L.D. Gulay; D. Kaczorowski; V.Ya. Shemet;
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正文语种 eng
中图分类合金学与各种性质合金;
关键词
Rare earth compounds; Chalcogenides; Crystal structures; X-ray single crystal diffraction; Magnetic properties;

机译：稀土化合物;硫属元素化物;晶体结构;X射线单晶衍射;磁性;

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Crystal structure of Ho_6Pb_9Se_(11) and magnetic properties of R_6Pb_2Se_(11) (R = Y, Dy and Ho)

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