Synthesis and X-ray structure of 11-N-benzylamido-9, 10-dihydro-9, 10-ethenoanthracene

Andrzej Fruzinski; Janina Karolak-Wojciechowska; Sandrine Alibert-Franco; Christiane Santelli-Rouvier; Jacques Barbe

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Synthesis and X-ray structure of 11-N-benzylamido-9, 10-dihydro-9, 10-ethenoanthracene

机译：11-N-苄基氨基-9、10-二氢-9、10-乙炔基蒽的合成及X射线结构

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As a part of studies on MDR reversing agents, the structure of a benzylamido-9, 10-dihydro-9, 10-ethenoanthracene is reported: C_(24) H_(19) N O; orthorhombic; space group: Pca2_1; a = 9.214(2), b = 18.624(4), c = 10.170(2) A; 1745.2(6) A~3; Z = 4. The three nonplanar rings from the 9, 10-dihydro-9, 10-ethenoanthracene skeleton of the molecule adopt a boat conformation. The benzamide side-chain is extended (conformation, trans-trans-gauche), The molecules in the crystal are joined by infinite chains of H-bonds N14-H14...013.

机译：作为MDR逆转剂研究的一部分，报道了苄基酰胺基9、10-二氢-9、10-乙炔基蒽的结构：C_（24）H_（19）N O;斜方晶空间组：Pca2_1; a = 9.214（2），b = 18.624（4），c = 10.170（2）A; 1745.2（6）A〜3; Z =4。该分子的9、10-二氢-9、10-乙撑蒽骨架中的三个非平面环采用船形。苯甲酰胺侧链延伸（构象，反式-反式），晶体中的分子通过H键N14-H14 ... 013的无限链连接。

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来源
《Journal of chemical crystallography》 |1999年第11期|共4页
作者
Andrzej Fruzinski; Janina Karolak-Wojciechowska; Sandrine Alibert-Franco; Christiane Santelli-Rouvier; Jacques Barbe;
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正文语种 eng
中图分类晶体学;
关键词
dihydro-ethenoanthracene; amide; MDR; chemosensitizers;

机译：二氢雅典娜酸;酰胺;耐多药;化学增敏剂;

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1. Synthesis and X-ray structure of 11-N-benzylamido-9, 10-dihydro-9, 10-ethenoanthracene [J] . Andrzej Fruzinski, Janina Karolak-Wojciechowska, Sandrine Alibert-Franco, Journal of chemical crystallography . 1999,第11期

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Synthesis and X-ray structure of 11-N-benzylamido-9, 10-dihydro-9, 10-ethenoanthracene

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