Structure of (2, 2'-bipyridine)lead(II) saccharinate monohydrate

G. Jovanovski; A. Hergold-Brundic; O. Grupce; D. Matkovic-Calogovic

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Structure of (2, 2'-bipyridine)lead(II) saccharinate monohydrate

机译：（2，2'-联吡啶）糖精铅（II）一水合物的结构

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The structure of (2, 2'-bipyridine)lead(II) saccharinate monohydrate has been investigated by X-ray diffraction. The compound crystallizes in the monoclinic space group P2_1 with a = 22.903(7), b = 12.608(3), c = 8.682(2) A, #beta# = 96.76(3) deg, and Z = 4. The structure consists of Pb~(2+) cations, 2, 2'-bipyridine ligands, saccharinato anions and water molecules. The Pb~(2+) cation is surrounded by two O atoms and four N atoms. The two saccharinato ions are nonequivalent. The water molecule forms hydrogen bonds of O_W...O_(CO) [2.810(16) A] and O_W...O_(SO2) [2.893(16) A] type.

机译：通过X射线衍射研究了（2，2'-联吡啶）糖精铅（II）一水合物的结构。该化合物在单斜空间群P2_1 / n中以a = 22.903（7），b = 12.608（3），c = 8.682（2）A，＃beta＃= 96.76（3）度和Z = 4结晶。结构由Pb〜（2+）阳离子，2、2'-联吡啶配体，糖精阴离子和水分子组成。 Pb〜（2+）阳离子被两个O原子和四个N原子包围。两种糖离子是不等价的。水分子形成O_W ... O_（CO）[2.810（16）A]和O_W ... O_（SO2）[2.893（16）A]类型的氢键。

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《Journal of chemical crystallography》 |1999年第2期|共5页
作者
G. Jovanovski; A. Hergold-Brundic; O. Grupce; D. Matkovic-Calogovic;
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正文语种 eng
中图分类晶体学;
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structure; (2; 2'-bipyridine)lead(II) saccharinate monohydrate;

机译：结构;（2;2'-联吡啶）铅（II）糖精一水合物;

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1. Structure of (2, 2'-bipyridine)lead(II) saccharinate monohydrate [J] . G. Jovanovski, A. Hergold-Brundic, O. Grupce, Journal of chemical crystallography . 1999,第2期

机译：（2，2'-联吡啶）糖精铅（II）一水合物的结构
2. INFRARED SPECTRA OF PROTIATED AND DEUTERATED LEAD(II) 2,2'-BIPYRIDINE SACCHARINATO MONOHYDRATE [J] . Grupce O., Jovanovski G. Journal of Molecular Structure . 1997,第0期

机译：2,2'-双吡啶二糖SA糖（II）的去离子和去氢铅的红外光谱
3. SYNTHESES AND CHARACTERIZATION OF A NEW ONE-DIMENSIONAL POLYMER CONTAINING (mu-THIOCYANATE)(bpy)LEAD(II) MOLECULE AND NEW MIXED-ANION LEAD (II) COMPLEXES: CRYSTAL STRUCTURES OF [Pb(bpy)(SCN)_2]_n (byp=2,2'-BIPYRIDINE) AND [Pb(phen)_2(NO_3)_(0.7)(ClO_ [J] . ALI MORSALI, MAHMOD PAYEGHADER, SAIED SALEHI MONFARED Journal of Coordination Chemistry . 2003,第9期

机译：含（硫氰酸盐）（bpy）铅（II）和新型混合阴离子铅（II）的一维新型高分子的合成与表征：[Pb（bpy）（SCN）_2] _n的晶体结构byp = 2,2'-BIPYRIDINE）and [Pb（phen）_2（NO_3）_（0.7）（ClO_
4. Synthesis, Structures and Properties of Two New Three-dimensional Ce(III) Coordination Polymers with 2,2'-bipyridine-4,4'-dicarboxylic Acid [C] . Ruiping Zheng, Huiyuan Chen, Junjie He, International Conference on Advanced Engineering Materials and Technology . 2013

机译：用2,2'-硼烷-4,4'-二羧酸的两种新三维Ce（III）配位聚合物的合成，结构和性质
5. PART I: THE OXIDATION OF PROPANE AT A CATALYST-COATED ION-EXCHANGE MEMBRANE SOLVATED WITH TRIFLUOROMETHANE SULFONIC ACID MONOHYDRATE. PART II: THE USE OF LEAD AS AN ELECTRODE MATERIAL FOR ANALYTICAL PURPOSES. PART III: THE EFFECT OF BENZIL RADICAL ANION INTERMEDIATES ON THE ELECTROREDUCTION OF BENZIL. [D] . MACK, ROBERT FRANCIS. 1983

机译：第一部分：丙烷在三氟甲苯磺酸单羟基磺酸盐溶液中催化的离子交换膜上的氧化。第二部分：使用铅作为分析目的的电极材料。第三部分：苯自由基阴离子中间体对苯的电还原的影响。
6. (22′-Bipyridine-κ2 NN′)bis(4-hydroxybenzoato-κ2 OO′)lead(II) monohydrate [O] . Jun Dai, Juan Yang 2010

机译：（22-联吡啶-κ2 NN）双（4-羟基苯并-κ2 一水合OO）铅（II）
7. Crystal structures of tetramethylammonium (2,2′-bipyridine)tetracyanidoferrate(III) trihydrate and poly[[(2,2′-bipyridine-κ2N,N′)di-μ2-cyanido-dicyanido(μ-ethylenediamine)(ethylenediamine-κ2N,N′)cadmium(II)iron(II)] monohydrate] [O] . Songwuit Chanthee, Wikorn Punyain, Supawadee Namuangrak, 2016

机译：四甲基铵（2,2'-联吡啶）四氰合铁（III）三水合物和聚[[（2,2'-联吡啶-κ2N，N'）二-μ2-氰基 - 二氰基（μ-乙二胺）（乙二胺-κ2N）的晶体结构，N'）镉（II）铁（II）]一水合物]

Structure of (2, 2'-bipyridine)lead(II) saccharinate monohydrate

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