Chemical preparation and crystal structure of 6'-butoxy-2, 6-diamino-3, 3' azo-dipyridine monohydrate

Faouzi Hlel; Leila Smiri

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Chemical preparation and crystal structure of 6'-butoxy-2, 6-diamino-3, 3' azo-dipyridine monohydrate

机译：6'-丁氧基-2，6-二氨基-3，3'偶氮-二吡啶一水合物的化学制备和晶体结构

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Chemical preparation, X-ray single crystal, and calorimetric studies of C_(14)H_(18)N_6O centre dot H_2O are described. The compound crystallizes in the triclinic space group, P1-bar with unit cell dimensions: a = 6.2640(3), b = 10.9840(4), c = 12.2220(3) A, #alpha# = 105.03(2), #beta# = 96.96(2), #gamma# = 101.6(2) deg, V = 712.10(5) A~3, and Z = 2. The 6'-butoxy-2, 6-diamino-3, 3'-azo-dipyridine monohydrate structure is built up from organic layers parallel to the (120) plane linked via 0 - H...N bond.

机译：描述了化学制备，X射线单晶和C_（14）H_（18）N_6O中心点H_2O的量热研究。该化合物在三斜晶空间群中结晶，P1-bar的晶胞尺寸为：a = 6.2640（3），b = 10.9840（4），c = 12.2220（3）A，＃alpha＃= 105.03（2），#beta ＃= 96.96（2），＃gamma＃= 101.6（2）deg，V = 712.10（5）A〜3，Z = 2.6'-丁氧基-2，6-二氨基-3，3'-偶氮-二吡啶一水合物结构由平行于通过（0-H ... N）键连接的（120）平面的有机层构成。

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《Journal of chemical crystallography》 |1999年第6期|共4页
作者
Faouzi Hlel; Leila Smiri;
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正文语种 eng
中图分类晶体学;
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6'-butoxy-2; 6-diamino-3; 3' azo-dipyridine; x-ray structure; hydrogen bonds;

机译：6'-丁氧基-2;6-二氨基-3;3'偶氮二吡啶;X射线结构;氢键;

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Chemical preparation and crystal structure of 6'-butoxy-2, 6-diamino-3, 3' azo-dipyridine monohydrate

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