3D Solid-State Network from Hierarchical Supramolecular Self-Assembly of Transition Metal Complexes of Pyridine Based Ligand

Pramanik A; Das G

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3D Solid-State Network from Hierarchical Supramolecular Self-Assembly of Transition Metal Complexes of Pyridine Based Ligand

机译：吡啶基配体的过渡金属配合物的分层超分子自组装的3D固态网络

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The crystal structures of [Cu(py)(4)(ClO4)](ClO4) (1), [V(pic)(2)(OH)](NO3)(2) center dot H2O (2) and [Ni(H2O)(6)] [Ni(dpa)(2)] center dot 2H(2)O (3) [py = Pyridine, picH = Pyridine-2-carboxylic acid, dpaH(2) = Pyridine-2,6-dicarboxylic acid] was determined by single-crystal X-ray diffraction techniques. Solid-state structural analysis shows that all these complexes from extensive 3D network structure via supramolecular self-assembly. The crystal structures are stabilized by extended hydrogen bonding interactions. The complex 2 forms orange V2O5 micro spheroids when heated at similar to 400 degrees C for 6 h.

机译：[Cu（py）（4）（ClO4）]（ClO4）（1），[V（pic）（2）（OH）]（NO3）（2）中心点H2O（2）和[Ni]的晶体结构（H2O）（6）] [Ni（dpa）（2）]中心点2H（2）O（3）[py =吡啶，picH =吡啶-2-羧酸，dpaH（2）=吡啶-2,6 -二羧酸]通过单晶X射线衍射技术测定。固态结构分析表明，所有这些复合物都是通过超分子自组装从广泛的3D网络结构中获得的。晶体结构通过延长的氢键相互作用而稳定。当在类似于400摄氏度的温度下加热6小时时，复合物2形成橙色的V2O5微球体。

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《Journal of chemical crystallography》 |2009年第6期|共7页
作者
Pramanik A; Das G;
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正文语种 eng
中图分类晶体学;
关键词
3D networks; Supramolecular self-assembly; Hydrogen-bonding; Thermal studies; Transition metal complex;

机译：3D网络;超分子自组装;氢键;热学;过渡金属配合物;

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1. 3D Solid-State Network from Hierarchical Supramolecular Self-Assembly of Transition Metal Complexes of Pyridine Based Ligand [J] . Pramanik A, Das G Journal of chemical crystallography . 2009,第6期

机译：吡啶基配体的过渡金属配合物的分层超分子自组装的3D固态网络
2. New polyoxometalate-templated supramolecular networks based on transition metal ions and pyridine-N-oxide ligands [J] . Feng X.-J., Yao W., Luo M.-F., Inorganica Chimica Acta . 2011,第1期

机译：基于过渡金属离子和吡啶-N-氧化物配体的新型多金属氧酸盐为模板的超分子网络
3. Transition metal complexes with thiosemicarbazide-based ligands. Part 46. Synthesis and physico-chemical characterization of mixed ligand cobalt(Ⅲ)-complexes with salicylaldehyde semi-, thiosemi- and isothiosemicarbazone and pyridine [J] . VUKADIN M. LEOVAC, LJILJANA S. VOJINOVIC, KATALIN MESZAROS SZECSENYI, Journal of the Serbian Chemical Society . 2003,第12期

机译：过渡金属配合物与基于硫代氨基脲的配体。第46部分。水杨醛半，硫代半和异硫代半碳脲和吡啶的混合配体钴（Ⅲ）-配合物的合成和理化性质
4. Hierarchical Self-Assembly of Block Copolymer Micelles Directed by Metal- Ligand Complexes [C] . Pierre Guillet, Clement Mugemana, Ulrich S. Schubert PMSE Symposia . 2009

机译：由金属配体配合物指导的嵌段共聚物胶束的分层自组装
5. Bis(thiophenolate)pyridine Pincer Ligands and Trivalent Zirconocene Complexes Relevant to Early Transition Metal Polymerization Catalysts. [D] . Lenton, Taylor. 2014

机译：与早期过渡金属聚合催化剂有关的双（硫酚盐）吡啶钳配体和三价锆茂配合物。
6. Supramolecular Chemistry And Self-assembly Special Feature: Anion-templated self-assembly of tetrahedral cage complexes ofcobalt(II) with bridging ligands containing two bidentatepyrazolyl-pyridine binding sites [O] . Rowena L. Paul, Zöe R. Bell, John C. Jeffery, 2002

机译：超分子化学和自组装特征：阴离子模板的四面体笼状配合物自组装含两个二齿桥联配体的钴（II）吡唑基-吡啶结合位点
7. Stimuli-Responsive Supramolecular Gels Constructed by Hierarchical Self-Assembly Based on Metal-Ligand Coordination and Host-Guest Recognition [O] . Yin-Hsuan Lee, Lipeng He, Yi-Tsu Chan 2018

机译：基于金属配体协调和宿主识别构建的刺激响应超分子凝胶。

3D Solid-State Network from Hierarchical Supramolecular Self-Assembly of Transition Metal Complexes of Pyridine Based Ligand

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