A polymer-supported (1,3,2)oxazaphospholidine for the conversion of isothiocyanates to isocyanides and their subsequent use in an ugi reaction.

Ley SV; Taylor SJ

首页> 外文期刊>Bioorganic and Medicinal Chemistry Letters >A polymer-supported (1,3,2)oxazaphospholidine for the conversion of isothiocyanates to isocyanides and their subsequent use in an ugi reaction.

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A polymer-supported (1,3,2)oxazaphospholidine for the conversion of isothiocyanates to isocyanides and their subsequent use in an ugi reaction.

机译：聚合物负载的（1,3,2）氮杂磷酰基吡啶，用于将异硫氰酸酯转化为异氰酸酯，并将其随后用于ugi反应中。

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摘要

The design and synthesis of a new polymer supported reagent for the clean conversion of isothiocyanates to isocyanides under microwave conditions was accomplished. The structurally diverse isocyanides generated were used in an Ugi 3CC, allowing the rapid generation of 2-isoindolinone-7-carboxamide analogues.

机译：完成了在微波条件下将异硫氰酸酯干净转化为异氰酸酯的新型聚合物负载试剂的设计和合成。在Ugi 3CC中使用了生成的结构多样的异氰化物，可快速生成2-isoindolinone-7-羧酰胺类似物。

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《Bioorganic and Medicinal Chemistry Letters》 |2002年第14期|共4页
作者
Ley SV; Taylor SJ;
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正文语种 eng
中图分类药学;生物化学;
关键词
Cyanides; Indoles; Isothiocyanates; Lactones; Organophosphorus Compounds; 氰化物; 吲哚类; 异硫氰酸盐类; 内酯类; 有机磷化合物; 恶唑类; 聚合物;

机译：Cyanides;Indoles;Isothiocyanates;Lactones;Organophosphorus Compounds;氰化物;吲哚类;异硫氰酸盐类;内酯类;有机磷化合物;恶唑类;聚合物;

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1. A polymer-supported (1,3,2)oxazaphospholidine for the conversion of isothiocyanates to isocyanides and their subsequent use in an ugi reaction. [J] . Ley SV, Taylor SJ Bioorganic and Medicinal Chemistry Letters . 2002,第14期

机译：聚合物负载的（1,3,2）氮杂磷酰基吡啶，用于将异硫氰酸酯转化为异氰酸酯，并将其随后用于ugi反应中。
2. Stereoselective P-Cyclisation and Diastereoisomeric Purification of 5-Phenyl-3-(pyridin-2-yl)-1,3,2-oxazaphospholidine Formed from a Thermolabile Protecting Group [J] . Kaczynski Tomasz P., Manszewski Tomasz, Chmielewski Marcin K. European journal of organic chemistry . 2016,第14期

机译：由不耐热保护基团形成的5-苯基-3-（吡啶-2-基）-1,3,2-氧杂磷腈的立体选择性P-环化和非对映异构体纯化
3. 4-Dimethylaminopyridine-catalyzed dynamic kinetic resolution in asymmetric synthesis of P-chirogenic 1,3,2-oxazaphospholidine-2-oxides [J] . Wang Lanlan, Cao Shanshan, Du Zhijun, RSC Advances . 2016,第92期

机译：4-二甲基氨基吡啶催化的P-蜂鸣1,3,2-恶唑磷苷-2-氧化物在不对称合成中的动态动力学分辨率
4. Ultrafast internal conversion cascade and subsequent photofragmentation of XUV excited caffeine molecule [C] . Kaoru Yamazaki 日本化学会春季年会講演予稿集 . 2018

机译：超快内部转换级联和随后的XUV激发咖啡因分子的光折叠
5. New convertible isocyanides for the Ugi reaction; application to the stereoselective synthesis of omuralide. [D] . Gilley, Cynthia Brooke. 2008

机译：用于Ugi反应的新型可转换异氰酸酯；在奥莫利特的立体选择性合成中的应用。
6. Synthesis of a novel category of pseudo-peptides using an Ugi three-component reaction of levulinic acid as bifunctional substrate amines and amino acid-based isocyanides [O] . Maryam Khalesi, Azim Ziyaei Halimehjani, Jürgen Martens 2019

机译：使用乙酰丙酸的乌吉三组分反应作为双功能底物胺和氨基酸基异氰酸酯合成新型伪肽
7. Synthesis of Optically Active 1,3,2-Oxazaphospholidine 2-Sulfides and 1,3,2-Benzodioxaphosphorin 2-Sulfides [O] . Shao-Yong Wu, Akinori Hirashima, Eiichi Kuwano, 1987

机译：合成光学活性的1,3,2-恶亚磷磷脂2-硫化物和1,3,2-苯并二磷素2-硫化物

A polymer-supported (1,3,2)oxazaphospholidine for the conversion of isothiocyanates to isocyanides and their subsequent use in an ugi reaction.

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