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Surface alteration of human tooth enamel subjected to acidic and neutral 30% hydrogen peroxide.

机译:人牙釉质的表面蚀变,在酸性和中性30%过氧化氢作用下进行。

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OBJECTIVES: To investigate the effects of acidic and neutral 30% hydrogen peroxide (HP) on human tooth enamel in terms of chemical structure, mechanical property, surface morphology and tooth colour. METHODS: Twenty-seven human dental blocks were obtained from premolars and randomly divided into three groups (n=9): Group acidic HP (30% HP, pH approximately 3.6), Group neutral HP (30% HP, pH approximately 7.0) and Group DW (distilled water, pH approximately 6.8). Attenuated total reflection-Fourier transform infrared spectroscopy (ATR-FTIR), Raman spectroscopy, atomic force microscopy (AFM) investigation, microhardness test and colour measurements were carried out before and after treatments. ATR-FTIR and Raman spectroscopy were analysed and then the carbonate:mineral ratio (C:M), Raman absolute intensity (RAI), Raman relative intensity (RRI), and laser-induced fluorescence intensity (FI) were obtained for evaluation. RESULTS: The C:M, percentage microhardness and percentage RRI of group acidic HP decreased more significantly than those of group neutral HP (P=0.02, P=0.001, P<0.001, respectively) and group DW (P=0.01, P=0.008, P<0.001, respectively). Whilst group neutral HP and group DW had no statistical difference in above terms (P=0.818, P=0.528, P=0.158, respectively). Significant morphological alterations were observed in group acidic HP. Group acidic HP and neutral HP had no significant difference in percentage FI (P=0.652) and DeltaE (P=0.906). CONCLUSIONS: This study suggested that neutral 30% HP had the same efficiency in tooth bleaching and it caused less deleterious effects on enamel than acidic 30% HP.
机译:目的:从化学结构,力学性能,表面形态和牙齿颜色等方面研究酸性和中性的30%过氧化氢(HP)对人牙釉质的影响。方法:从前磨牙获得二十七个人类牙齿块,并将其随机分为三组(n = 9):酸性HP组(30%HP,pH约3.6),中性HP组(30%HP,pH约7.0)和DW组(蒸馏水,pH约6.8)。在处理前后进行了衰减全反射傅里叶红外光谱(ATR-FTIR),拉曼光谱,原子力显微镜(AFM)研究,显微硬度测试和颜色测量。分析了ATR-FTIR和拉曼光谱,然后获得碳酸盐:矿物比(C:M),拉曼绝对强度(RAI),拉曼相对强度(RRI)和激光诱导的荧光强度(FI)进行评估。结果:酸性HP组的C:M,显微硬度百分比和RRI百分比分别比中性HP组(P = 0.02,P = 0.001,P <0.001)和DW组(P = 0.01,P = 0.008,P <0.001)。而中性HP组和DW组在上述各项方面无统计学差异(分别为P = 0.818,P = 0.528,P = 0.158)。在酸性HP组中观察到明显的形态学改变。酸性HP组和中性HP组的FI百分比(P = 0.652)和DeltaE百分比(P = 0.906)没有显着差异。结论:这项研究表明,中性的30%HP具有与酸性的30%HP相同的牙齿漂白效率,并且对牙釉质的有害影响较小。

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