On-plate spot test for identification and separation of benzalkonium chloride and cetrimide in drug samples: A mechanistic view

Ali Mohammad; Asma Siddiq; Rizwana Mobin

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On-plate spot test for identification and separation of benzalkonium chloride and cetrimide in drug samples: A mechanistic view

机译：板载斑点测试用于鉴定和分离药物样品中的苯扎氯铵和西曲美德：机理性观点

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A mechanism showing different modes of interaction of benzalkonium chloride and cetrimide with the stationary and mobile phase has been proposed which leads to the separation of this surfactant mixture. Other combination of cationic surfactants was also separated from their binary mixture by the chromatographic system comprising of silica gel and combination of green solvents as mobile phase. The effect of presence of impurities on separation process was also examined and the limits of detection of the separated surfactants were calculated. The developed method was also successfully applied for the identification of cetrimide and benzalkonium chloride in pharmaceutical formulations.

机译：已经提出了一种机理，该机理显示了苯扎氯铵和西曲美铵与固定相和流动相的不同相互作用方式，这导致该表面活性剂混合物的分离。阳离子表面活性剂的其他组合也可以通过色谱系统从其二元混合物中分离出来，该色谱系统包括硅胶和绿色溶剂的组合作为流动相。还检查了杂质的存在对分离过程的影响，并计算了分离出的表面活性剂的检出限。所开发的方法也成功地用于药物制剂中西曲美肽和苯扎氯铵的鉴定。

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《Journal of industrial and engineering chemistry》 |2014年第4期|共6页
作者
Ali Mohammad; Asma Siddiq; Rizwana Mobin;
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正文语种 eng
中图分类化学工业;
关键词
Separation; Benzalkonium chloride; Cetrimide; Densitometry; Pharmaceutical formulations;

机译：分离;苯扎氯铵;西曲美特;光密度法;药物制剂;

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1. On-plate spot test for identification and separation of benzalkonium chloride and cetrimide in drug samples: A mechanistic view [J] . Ali Mohammad, Asma Siddiq, Rizwana Mobin Journal of industrial and engineering chemistry . 2014,第4期

机译：板载斑点测试用于鉴定和分离药物样品中的苯扎氯铵和西曲美德：机理性观点
2. Allergy to benzalkonium chloride in plaster of Paris after sensitisation to cetrimide. A case report [J] . P Staniforth The Journal of Bone and Joint Surgery. British VolumecBritish Orthopaedic Association , Australian Orthopaedic Association , Canadian Orthopaedic Association . . . [et al] . 1980,第4期

机译：塞西米德致敏后，对巴黎石膏中的苯扎氯铵过敏。病例报告
3. Combining poly(dimethyldiphenylsiloxane) and nitrile phases for improving the separation and quantitation of benzalkonium chloride homologues: In-tube solid phase microextraction-capillary liquid chromatography-diode array detection-mass spectrometry for analyzing industrial samples [J] . Prieto-Blanco M.C., Moliner-Martinez Y., Campíns-Falcó P. Journal of chromatography, A: Including electrophoresis and other separation methods . 2013,第Null期

机译：结合使用聚二甲基二苯基硅氧烷和腈相以改善苯扎氯铵同系物的分离和定量：管内固相微萃取-毛细管液相色谱-二极管阵列检测-质谱法分析工业样品
4. Characterization of a Selective Androgen Receptor Modulator Drug Candidate and Identification of In Vitro Generated Metabolites for Sports Drug Testing [C] . Mario Thevis, Andreas Lagojda, Andreas Thomas, ASMS Conference on Mass Spectrometry and Allied Topics . 2015

机译：一种选择性雄激素受体调节剂药物候选药物候选药物候选的表征及体外生成代谢物的体育药物检测
5. Adulterants and interpretive challenges in forensic science: Effects on colorimetric spot tests for presumptive drug identification and adverse side effects in the body. [D] . Cosby, Daniel A. 2014

机译：法医科学中的掺假剂和解释性挑战：对比色斑点检测的影响，以用于推定药物的鉴定和对人体的不良副作用。
6. Toxicity of antiglaucoma drugs with and without benzalkonium chloride to cultured human corneal endothelial cells [O] . Masahiko Ayaki, Atsuo Iwasawa, Yoichi Inoue 2010

机译：含或不含苯扎氯铵的抗青光眼药物对培养的人角膜内皮细胞的毒性
7. Allergy to benzalkonium chloride in plaster of Paris after sensitisation to cetrimide. A case report [O] . P Staniforth 1980

机译：敏化后对巴黎甲基氯化锡的过敏症对环纤维。案例报告

On-plate spot test for identification and separation of benzalkonium chloride and cetrimide in drug samples: A mechanistic view

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