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Precipitation-deposition assisted fabrication and characterization of nano-sized zinc manganite

机译:沉淀沉积辅助纳米锰锌矿的制备与表征

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摘要

Catalytic and structural investigations of nano-sized zinc manganite (ZnMn2O4) powders have been determined. These manganites were prepared by precipitation-deposition route followed by heating at 400, 600, and 800 °C. The final products were characterized X-ray diffraction, scanning electron microscopy (SEM), transmission electron microscopy (TEM), and energy dispersive X-ray (EDX). The catalytic activity of the as prepared systems was measured by the hydrogen peroxide decomposition in aqueous solution over the solid surface at 30-50 °C. The results showed that the calcination temperature affects the different characteristics of the investigated solids.
机译:已经确定了纳米级锰酸锌(ZnMn2O4)粉末的催化和结构研究。这些锰矿是通过沉淀-沉积路线,然后在400、600和800°C下加热制备的。最终产品经过X射线衍射,扫描电子显微镜(SEM),透射电子显微镜(TEM)和能量色散X射线(EDX)表征。通过在30-50℃下在固体表面上的水溶液中的过氧化氢分解来测量所制备系统的催化活性。结果表明,煅烧温度影响所研究固体的不同特性。

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