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首页> 外文期刊>Journal of industrial and engineering chemistry >Multiwalled carbon nanotube impregnated with tartrazine: Solid phase extractant for Cd(II) and Pb(II)
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Multiwalled carbon nanotube impregnated with tartrazine: Solid phase extractant for Cd(II) and Pb(II)

机译:酒石黄浸渍的多壁碳纳米管:Cd(II)和Pb(II)的固相萃取剂

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摘要

A solid phase extraction procedure has been presented by using multiwalled carbon nanotube impregnated with tartrazine for cadmium (Cd(II)) and lead (Pb(II)) ions. The influences of pH, flow rate, eluent and sample volume were investigated. No interference effects were observed from the alkaline, alkaline earth and some transition metals. The detection limits (LOD) were 0.8 and 6.6 μg L~(-1) for Cd(Il) and Pb(II), respectively. The preconcentration factor was 40. The validation of the procedure was controlled by the analysis of certified references materials. The procedure was applied to the determination of cadmium and lead in natural water and food samples.
机译:提出了一种通过使用酒石黄浸渍的多壁碳纳米管获得镉(Cd(II))和铅(Pb(II))离子的固相萃取程序。研究了pH,流速,洗脱液和样品量的影响。没有观察到碱金属,碱土金属和某些过渡金属的干扰作用。 Cd(II)和Pb(II)的检出限(LOD)分别为0.8和6.6μgL〜(-1)。预浓缩系数为40。通过对标准参考物质的分析来控制程序的有效性。该方法用于测定天然水和食品样品中的镉和铅。

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