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Auto-combustion preparation and characterization of BaFe12O19 nanostructures by using maleic acid as fuel

机译:马来酸为燃料的BaFe12O19纳米结构的自动燃烧制备及表征

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In this paper, barrium hexaferrite nanoparticles have been successfully synthesized via sal-gel auto combustion method based on the reaction between Ba(NO3)(2) and Fe(NO3)(3) in water, in present of maleic acid as capping agent and fuel. Also, various polymers used to obtaining pure phase barrium hexaferrite. The products were characterized by X-ray diffraction, scanning electron microscopy, X-ray energy dispersive spectroscopy analysis. To investigate the effects of amount of maleic acid and the kind of polymer on the morphology of products and finding optimal condition, several experiments were carried out. It was found that the phase and morphology of products could be influenced by these parameters. Vibrating sample magnetometer (VSM) was used to study the magnetism properties of BaFe12O19 samples. (C) 2014 The Korean Society of Industrial and Engineering Chemistry. Published by Elsevier B.V. All rights reserved.
机译:本文在水体中Ba(NO3)(2)与Fe(NO3)(3)之间的反应,马来酸作为封端剂和水的反应条件下,通过Sal-gel自动燃烧法成功合成了六价铁酸钡纳米粒子。汽油。另外,用于获得纯相六铁酸钡的各种聚合物。通过X射线衍射,扫描电子显微镜,X射线能量色散光谱分析对产物进行表征。为了研究马来酸的量和聚合物的种类对产品形态的影响并找到最佳条件,进行了一些实验。发现这些参数可能影响产物的相和形态。振动样品磁力计(VSM)用于研究BaFe12O19样品的磁性。 (C)2014大韩工业化学工程学会。由Elsevier B.V.发布。保留所有权利。

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