Effective methods for the measurement of CsI cluster ions using MALDI-MS with suitable solvent combinations and additives

Shunsuke Mochizuki

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Effective methods for the measurement of CsI cluster ions using MALDI-MS with suitable solvent combinations and additives

机译：使用MALDI-MS与合适的溶剂组合和添加剂一起测量CsI簇离子的有效方法

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method to measure CsI cluster ions ((CsI)_nCs~+, (CsI)_nI~-) from CsI samples in matrix-assisted laser desorption/ionization mass spectrometry (MALDI-MS) was developed with a 2-[(2E)-3-(4-tert-butylphenyl)-2-methylprop-2-enylidene] malononitrile (DCTB) matrix and additives. Solvent combinations in which the CsI and DCTB solutions were miscible were effective in detecting CsI cluster ions at amass range of over m/z 2000 and are associated with a characteristic spread of DCTB within the CsI/DCTB mixture. The addition of saccharides or sugar alcohols to the CsI/DCTB mixture improved the DCTB distribution and widened the mass distribution of CsI cluster ions up to m/z 10 000 in the linear mode.

机译：用2-[（（2E）- 3-（4-叔丁基苯基）-2-甲基丙-2-烯基]丙二腈（DCTB）基质和添加剂。 CsI和DCTB溶液可混溶的溶剂组合有效检测ms / z 2000以上质量范围的CsI簇离子，并且与DCs在CsI / DCTB混合物中的特征扩散有关。在线性模式下，向CsI / DCTB混合物中添加糖类或糖醇可改善DCTB分布，并将CsI簇离子的质量分布扩大至m / z 10000。

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来源
《Journal of mass spectrometry: JMS》 |2014年第11期|共4页
作者
Shunsuke Mochizuki;
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正文语种 eng
中图分类分析化学;
关键词
CsI cluster ion; DCTB; solvent; saccharide; MALDI mass spectrometry;

机译：CsI簇离子;DCTB;溶剂;糖;MALDI质谱;

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1. Effective methods for the measurement of CsI cluster ions using MALDI-MS with suitable solvent combinations and additives [J] . Shunsuke Mochizuki Journal of mass spectrometry: JMS . 2014,第11期

机译：使用MALDI-MS与合适的溶剂组合和添加剂一起测量CsI簇离子的有效方法
2. Enhanced measurement of CsI cluster ions for mass calibration in MALDI-MS using sugar alcohols [J] . Mochizuki Shunsuke Analytical methods . 2015,第5期

机译：使用糖醇在MALDI-MS中进行质量校准时增强CsI簇离子的测量
3. Enhanced measurement of CsI cluster ions for mass calibration in MALDI-MS using sugar alcohols [J] . Shunsuke Mochizuki Analytical methods . 2015,第5期

机译：使用糖醇在MALDI-MS中进行质量校准的CsI簇离子的增强测量
4. Determination System of Single Tuition Group Using a Combination of Fuzzy C-Means Clustering and Simple Additive Weighting Methods [C] . Indrawati, Anwar, Nova Amalia International Conference on Science and Innovated Engineering . 2019

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5. Solvent methods in coupled-cluster theory. [D] . Thanthiriwatte, Kanchana Sahan. 2009

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7. Fractionation and Solvent-Free MALDI-MS Analysis of Polymers Using Liquid Adsorption Chromatography at Critical Conditions of Adsorption in Combination with a Multisample On-Target Homogenization/Transfer Sample Preparation Method [O] . -1

机译：使用液体吸附色谱法在吸附临界条件下使用液体吸附色谱法分析聚合物的分馏和无溶剂MALDI-MS分析，与多样的均质均质化/转移样品制备方法组合
8. Configurational Energies in Terms of Effective Cluster Interactions in Binary Substitutional Alloys: Connection Between the Embedded Cluster Method and the Generalized Perturbation Method [R] . Turchi, P. E. A. , Gonis, A. , Zhang, X. , 1987

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Effective methods for the measurement of CsI cluster ions using MALDI-MS with suitable solvent combinations and additives

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