Biaxial orientation mechanism of drawn natural rubber. III. Determination of the orientation function from wide-angle x-ray diffraction pattern

Alam MM; Osaka H; Asano T

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Biaxial orientation mechanism of drawn natural rubber. III. Determination of the orientation function from wide-angle x-ray diffraction pattern

机译：拉伸天然橡胶的双轴取向机理。三，从广角X射线衍射图确定取向函数

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Biaxial orientation (BO) was observed during the uniaxial drawing of bulk natural rubber (NR). The degree of BO was compared in NR films named TCL-0 and TCL-1, having original widths of 1mm and 8mm, respectively. The results of wide-angle X-ray diffraction (WAXD) indicated that BO was enhanced with increasing film width. The degree of BO was quantitatively evaluated by an orientation function of the (200) plane, F-200. We proposed a new method to evaluate F-200 using an intensity ratio (R) of 120 and 200 reflections. For this purpose, a theoretical relation of R versus F-200 was calculated using Gaussian and/or Lorentzian distribution functions. Following the new method, we obtained 0.06

机译：在块状天然橡胶（NR）的单轴拉伸过程中观察到双轴取向（BO）。在原始膜宽分别为1mm和8mm的NR膜TCL-0和TCL-1中比较了BO的程度。广角X射线衍射（WAXD）的结果表明，BO随着膜宽度的增加而增强。 BO的程度通过（200）面的取向函数F-200进行定量评价。我们提出了一种使用120和200次反射的强度比（R）评估F-200的新方法。为此，使用高斯和/或洛伦兹分布函数计算了R对F-200的理论关系。按照新方法，取决于伸长后的样品宽度，对于TCL-0，我们获得0.06

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《Journal of Macromolecular Science. Physics》 |2008年第2期|共21页
作者
Alam MM; Osaka H; Asano T;
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正文语种 eng
中图分类分子物理学;
关键词
natural rubber; wide-angle X-ray diffraction; biaxial orientation; free space model; STRESS-INDUCED CRYSTALLIZATION; THIN-FILMS; MOLECULAR-ORIENTATION; POLYCHLOROPRENE; STRAIN; DEFORMATION; MORPHOLOGY; PROPERTY; TEM;

机译：天然橡胶;广角X射线衍射;双轴取向;自由空间模型;应力诱导结晶;薄膜;分子取向;聚氯丁二烯;应变;形变;形态学;性能;TEM;

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1. Biaxial orientation mechanism of drawn natural rubber. III. Determination of the orientation function from wide-angle x-ray diffraction pattern [J] . Alam MM, Osaka H, Asano T Journal of Macromolecular Science. Physics . 2008,第2期

机译：拉伸天然橡胶的双轴取向机理。三，从广角X射线衍射图确定取向函数
2. Biaxial orientation mechanism of drawn natural rubber. III. Determination of the orientation function from wide-angle x-ray diffraction pattern [J] . Alam MM, Osaka H, Asano T Journal of Macromolecular Science. Physics . 2008,第2期

机译：拉伸天然橡胶的双轴取向机理。三，从广角X射线衍射图确定取向函数
3. Biaxial Orientation Mechanism of Drawn Natural Rubber. III. Determination of the Orientation Function from Wide-Angle X-Ray Diffraction Pattern [J] . Journal of Macromolecular Science, Part B . 2008,第2期

机译：拉伸天然橡胶的双轴取向机理。三，从广角X射线衍射图确定取向函数
4. WIDE-ANGLE X-RAY DIFFRACTION STUDY OF AMORPHOUS ORIENTATION AND AMORPHOUS AGGREGATES IN POLYMERS (Paper No. 34) [C] . Lizhi Liu, Tzu-Chi Kuo, David Henton, Spring 2005 167th Technical Meeting of the Rubber Division, American Chemical Society(ACS) . 2005

机译：聚合物中无规取向和无规聚集体的广角X射线衍射研究（第34号论文）
5. Solving virus structures from xfel diffraction patterns of random particle orientations using angular correlations of intensities [D] . Uddin, Miraj. 2013

机译：使用强度角度相关性从随机粒子方向的xfel衍射图样求解病毒结构
6. The correlation of single-particle diffraction patterns as a continuous function of particle orientation [O] . Andrew V. Martin 2014

机译：单粒子衍射图的相关性是粒子取向的连续函数
7. A wide-angle X-ray fibre diffraction method for quantifying collagen orientation across large tissue areas: application to the human eyeball coat [O] . Pijanka, JK, Abass, A, Sorensen, T, 2013

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8. Determination of Crystallite Orientation Distribution Functions (CODF) and Their Use in Surface Texture Analysis Using X-ray Diffraction [R] . Jones, A. M. 1988

机译：微晶取向分布函数（CODF）的测定及其在X射线衍射表面纹理分析中的应用

Biaxial orientation mechanism of drawn natural rubber. III. Determination of the orientation function from wide-angle x-ray diffraction pattern

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