Poly(3,5-dichloroaniline) Doped with Different Sulfonic Acids

Fernando R. Diaz; Jorge L. Torres; M. Angelica Del Valle; Jorge H. Velez; J. Christian BernEde; Gaston A. East

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Poly(3,5-dichloroaniline) Doped with Different Sulfonic Acids

机译：掺杂有不同磺酸的聚（3,5-二氯苯胺）

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Poly(3,5-dichloroaniline) was prepared by chemical oxidation in the presence of various sulfonic acids as doping agent, using potassium permanganate as oxidant. 1-Naphtalene sulfonic acid, 2-naphatalene sulphonic acid, 1,5-naphtalene disulfonic acid, and p-toluenesulfonic acid were the acids of choice. Infrared and UV-Vis spectroscopy, utilized to characterize the polymers, revealed that the compounds exist in the emeraldine (conductive) oxidation state. The level of doping, conductivity, and morphology were determined as well. The presence of a sulfonic acid produces a morphological change, from granular to microtubule structures, which is responsible for the strong increase in the conductivity of the polymer.

机译：使用高锰酸钾作为氧化剂，在各种磺酸作为掺杂剂的存在下，通过化学氧化法制备了聚（3,5-二氯苯胺）。选择的是1-萘磺酸，2-萘磺酸，1,5-萘二磺酸和对甲苯磺酸。用于表征聚合物的红外光谱和紫外可见光谱表明，这些化合物以翡翠（导电）氧化态存在。还确定了掺杂水平，电导率和形态。磺酸的存在会产生从粒状到微管结构的形态变化，这是导致聚合物电导率大幅提高的原因。

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《Journal of Macromolecular Science. Pure and Applied Chemistry》 |2007年第12期|共8页
作者
Fernando R. Diaz; Jorge L. Torres; M. Angelica Del Valle; Jorge H. Velez; J. Christian BernEde; Gaston A. East;
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正文语种 eng
中图分类高分子化学（高聚物）;
关键词
chemical oxidation; sulfonic acids; polymer conductivity; doping agent; potassium permanganate;

机译：化学氧化;磺酸;聚合物电导率;掺杂剂;高锰酸钾;

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1. Poly(3,5-dichloroaniline) Doped with Different Sulfonic Acids [J] . Fernando R. Diaz, Jorge L. Torres, M. Angelica Del Valle, Journal of Macromolecular Science. Pure and Applied Chemistry . 2007,第10a12期

机译：掺杂有不同磺酸的聚（3,5-二氯苯胺）
2. STRUCTURES AND PROPERTIES OF THE WATER-SOLUBLE SELF-ACID-DOPED CONDUCTING POLYMER BLENDS - SULFONIC ACID RING-SUBSTITUTED POLYANILINE/POLY(VINYL ALCOHOL) AND POLY(ANILINE-CO-N-PROPANESULFONIC ACID ANILINE)/POLY(VINYL ALCOHOL) [J] . Chen SA., Hwang GW. Polymer: The International Journal for the Science and Technology of Polymers . 1997,第13期

机译：水溶性自掺杂导电聚合物共混物的结构和性能-磺胺酸环取代的聚苯胺/聚乙烯醇（乙烯醇）和聚（苯胺-CO-N-丙炔醇苯胺）/聚乙烯醇（乙烯醇）
3. p-Doping of poly(3-hexylthiophene-2,5-diyl) with sulfonic acids and oxygen related to self-doping of sulfonated polythiophenes [J] . Takakazu Yamamoto Chemistry Letters . 2003,第4期

机译：用磺酸和氧对聚（3-己基噻吩-2,5-二基）进行p掺杂与磺化聚噻吩的自掺杂有关
4. Addition effect of aliphatic monools and diols on the conductivity enhancement of poly(3,4-ethylenedioxythiophene) doped with poly(styrene sulfonic acid) (PEDOT:PSS) [C] . Shigeji Konagaya, Misako Mutou, Mariko Terada International Conference of the Polymer Processing Society . 2019

机译：脂族金属脂族金属和二醇对聚（苯乙烯磺酸）（PEDOT：PSS）掺杂聚（3,4-亚乙基氧噻吩）的电导率增强的添加效果
5. A new class of polyelectrolytes, poly(phenylene sulfonic acids) and its copolymers as proton exchange membranes for PEMFC's. [D] . Granados-Focil, Sergio. 2006

机译：新型的聚电解质，聚苯磺酸及其共聚物，可作为PEMFC的质子交换膜。
6. Processable dodecylbenzene sulfonic acid (DBSA) doped poly(N-vinyl carbazole)-poly(pyrrole) for optoelectronic applications [O] . W. A. Hammed, M. S. Rahman, H. N. M. E. Mahmud, 2017

机译：用于光电应用的可加工的十二烷基苯磺酸（DBSA）掺杂的聚（N-乙烯基咔唑）-聚（吡咯）
7. Processable dodecylbenzene sulfonic acid (DBSA) doped poly(N-vinyl carbazole)-poly(pyrrole) for optoelectronic applications [O] . W. A. Hammed, M. S. Rahman, H. N. M. E. Mahmud, 2016

机译：可加工的十二烷基苯磺酸（DBSA）掺杂聚（N-乙烯基咔唑）-poly（吡咯）用于光电应用
8. Initial Submission: 3,5-dimethyl-4-hydroxyphenyl Sulfonic Acid: Subacute Dermal & Oral Toxicity Studies in Albino Rabbits and Hairless Mice with Cover Sheets & Letter dated 060592. [R] . 1992

机译：初始提交：3,5-二甲基-4-羟基苯基磺酸：白蛋白兔和无毛小鼠的亚急性皮肤和口腔毒性研究，带有封面和060592的信函。

Poly(3,5-dichloroaniline) Doped with Different Sulfonic Acids

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