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Preparation of translucent barium titanate ceramics from sol-gel-derived transparent monolithic gels

机译:由溶胶凝胶衍生的透明整体凝胶制备半透明钛酸钡陶瓷

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摘要

Translucent barium titanate (BaTiO3) ceramics with a relative sintered density of 85% have been successfully produced via a powderless sol-gel method, in which transparent, partially-crystallized BaTiO3 monolithic xerogels (dried gels) were prepared and submitted to sintering at 1100 degrees C in an oxygen atmosphere. The transparent BaTiO3 xerogels turned opaque upon sintering at temperatures in the range 600 to 1000 degrees C, but sintering at 1100 degrees C resulted in the formation of translucent bodies. Pore size distribution measurements demonstrate that most pores present in the translucent materials are open pores with a diameter of < 10 nm. [References: 8]
机译:通过无粉溶胶-凝胶法成功地制备了相对烧结密度为85%的半透明钛酸钡(BaTiO3)陶瓷,其中制备了透明的,部分结晶的BaTiO3整体干凝胶(干燥的凝胶),并在1100度下进行了烧结。 C在氧气气氛中。透明的BaTiO3干凝胶在600到1000摄氏度的温度下烧结后变成不透明,但在1100摄氏度下烧结导致形成半透明物体。孔径分布测量结果表明,半透明材料中存在的大多数孔都是直径小于10 nm的开孔。 [参考:8]

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