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Chalcogenide nanowires by evaporation-condensation

机译:通过蒸发缩合的硫属化物纳米线

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Chalcogenide (arsenic sulfide) nanowires have been successfully synthesized front As2S1 under near-equilibrium conditions via an evaporation-condensation process in evacuated glass ampoules. The as-synthesized rianowires were pure, nearly stoichiometric, and amorphous. The nanowires had diameters ranging from 40 to 140 nm and lengths tip to a few millimeters. Distinct joints of the crisscrossing nanowires indicate potential for forming structural networks. They hake been characterized using scanning electron microscopy (SEM), transmission electron microscopy (TEM). energy dispersive spectroscopy (EDS). Raman spectroscopy, and X-ray diffraction (XRD) to determine their structure, composition. and morphology, Selected area diffraction (SAD) in the TEM and XRD confirmed their amorphous nature. The As-S nanowires could make in ideal system for understanding the carrier transport and photonic properties in nanoscale for this family of materials (IV V compounds), Chalcogenide nanowires show promise for integrated nanoelectronics and biophotonics. (c) 2005 Elsevier B.V. All rights reserved.
机译:硫属元素化物(硫化砷)纳米线已通过在真空玻璃安瓿中通过蒸发-冷凝过程在接近平衡的条件下成功合成了正面As2S1。合成后的铁丝是纯净的,接近化学计量的和无定形的。纳米线的直径范围为40至140 nm,尖端的长度为几毫米。交叉的纳米线的不同接头表明形成结构网络的潜力。使用扫描电子显微镜(SEM),透射电子显微镜(TEM)对它们进行了表征。能量色散光谱(EDS)。拉曼光谱法和X射线衍射(XRD)确定其结构,组成。在形态和形态上,TEM和XRD中的选择区域衍射(SAD)证实了它们的非晶态性质。 As-S纳米线可以成为理想的系统,以了解该材料家族(IV V化合物)的纳米级载流子传输和光子特性,硫族化物纳米线显示出​​有望用于集成纳米电子学和生物光子学。 (c)2005 Elsevier B.V.保留所有权利。

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