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Electrolyte influence on the anodic synthesis of TiO2 nanotube arrays

机译:电解质对TiO2纳米管阵列阳极合成的影响

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摘要

We report on the structural and morphological features of self-aligned titanium oxide nanotube arrays grown by electrochemical anodization in different electrolytes comprising aqueous acidic media or organic neutral media, and at several potentiostatic voltages ranging between 12 and 60 V. The results show an improvement in the self-alignment of the nanotube arrays and an increase of about 10,000% in the nanotubes length obtained by anodization performed with NH4F in ethylene glycol electrolyte, respect to the case obtained employing the aqueous electrolytes.
机译:我们报告了通过在不同的电解质中(包括水性酸性介质或有机中性介质)进行电化学阳极氧化而生长的自对准氧化钛纳米管阵列的结构和形态学特征,并且在几种恒电位电压范围为12至60 V之间。相对于使用水性电解质获得的情况,通过使用NH 4 F在乙二醇电解质中进行阳极氧化获得的纳米管阵列的自对准和纳米管长度的增加约10,000%。

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