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A novel process to produce nanoporous aluminum oxide using titration technique to prepare the neutral electrolyte

机译:利用滴定技术制备中性电解质的纳米多孔氧化铝的新工艺

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摘要

A novel process is employed in the fabrication of porous anodic aluminum oxide film in neutral electrolyte. A titration technique which involves titration of acid-base neutralization process is used as the electrolyte source in the anodization of the aluminum substrate. Freshly prepared 10% phosphoric acid at pH1 is titrated with 1 M of sodium hydroxide until it reaches pH7 in a neutral environment. The growth of the porous anodic film was made possible by 60 V dc applied potential from an in-house electrochemical cell to the aluminum substrate in the neutral electrolyte. The diameter of the pores produced is in the range of 40-200 nm.
机译:在中性电解质中制造多孔阳极氧化铝膜中采用了一种新颖的方法。在铝基板的阳极氧化中,将涉及酸碱中和过程的滴定的滴定技术用作电解质源。将新鲜配制的pH1的10%磷酸用1 M氢氧化钠滴定,直到在中性环境中达到pH7。通过从内部电化学电池向中性电解质中的铝基板施加60 V dc的电势,可以使多孔阳极膜的生长。产生的孔的直径在40-200nm的范围内。

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