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Porous glass reinforced hydroxyapatite materials produced with different organic additives

机译:用不同的有机添加剂生产的多孔玻璃增强羟基磷灰石材料

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摘要

In the present study three different organic additives were used to produce porous structures of a CaO-P2O5 glass reinforced hydroxyapatite potato starch, almond crust and wax spheres. The produced samples were analysed by scanning electron microscopy, X-ray diffraction with Rietveld refinement, differential thermal analysis and mercury porosimetry. The techniques used in this study enabled the production of glass reinforced hydroxyapatite samples with various pore diameters. Two different techniques were used to produce porous glass reinforced hydroxyapatite samples: a dry method using wax spheres as pore formers and a wet method in alcoholic suspension, where almond crust and potato starch were used as pore formers. The final microstructure consists of hydroxyapatite, alpha-tricalcium phosphate and beta-tricalcium phosphate. X-ray diffraction and scanning electron microscopy analysis revealed different percentages of phases when comparing dense and porous glass reinforced hydroxyapatite specimens, These hard materials are intended to be used as bone defect fillers. (C) 2002 Elsevier Science B.V. All rights reserved. [References: 16]
机译:在本研究中,三种不同的有机添加剂被用于生产CaO-P2O5玻璃纤维增​​强的羟基磷灰石马铃薯淀粉,杏仁壳和蜡球的多孔结构。通过扫描电子显微镜,采用Rietveld精制的X射线衍射,差热分析和水银孔隙率法对生产的样品进行分析。这项研究中使用的技术能够生产具有各种孔径的玻璃纤维增​​强羟基磷灰石样品。两种不同的技术被用于生产多孔玻璃纤维增​​强羟基磷灰石样品:使用蜡球作为成孔剂的干法和在酒精悬浮液中的湿法,其中杏仁壳和马铃薯淀粉被用作成孔剂。最终的微观结构由羟基磷灰石,α-磷酸三钙和β-磷酸三钙组成。 X射线衍射和扫描电子显微镜分析显示,当比较致密和多孔的玻璃纤维增​​强羟基磷灰石样品时,相的百分比不同。这些硬质材料旨在用作骨缺损填充物。 (C)2002 Elsevier Science B.V.保留所有权利。 [参考:16]

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