SEPARATION AND IMPROVEMENT IN DETECTION OF POLYCYCLIC AROMATIC HYDROCARBONS BY REVERSE-PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHY USING MICELLAR MOBILE PHASE AND FLUORESCENCE DETECTOR

Hadjmohammadi MR; Fatemi MH

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SEPARATION AND IMPROVEMENT IN DETECTION OF POLYCYCLIC AROMATIC HYDROCARBONS BY REVERSE-PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHY USING MICELLAR MOBILE PHASE AND FLUORESCENCE DETECTOR

机译：反相液相色谱-荧光检测器反相高效液相色谱法检测和分离多环芳烃

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Separation and investigation of Detection Limit (LOD)of Polycyclic Aromatic Hydrocarbons,PAH,compounds with RP-HPLC using fluorescence detection were studied Lower LOD for these compounds were observed because of higher fluorescence intensity in the prescence of micellar mobile phase as compared to those of hydroorganics. The codition for optimum separation and enhancement of fluorescence intensity by variation of concentration of coorganic solvent (2-Propanol) and SDS were obtained. Selectivity factor and fluorescence intensity were the basic factors for the optimization of separation and improvement in detection respectively. The condition obtined were 3% of 2-Propanol in 0.035 M SDS.

机译：采用荧光检测的RP-HPLC对多环芳烃，PAH，化合物的检测限（LOD）进行了分离和研究，研究发现这些化合物的LOD较低，因为胶束流动相的发质的荧光强度高于水有机物。通过改变有机溶剂（2-丙醇）和SDS的浓度，获得了最佳分离和增强荧光强度的条件。选择性因子和荧光强度分别是优化分离和改善检测的基本因素。提出的条件是在0.035 M SDS中使用3％的2-丙醇。

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《Journal of Liquid Chromatography》 |1995年第13期|共10页
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Hadjmohammadi MR; Fatemi MH;
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正文语种 eng
中图分类分析化学;
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1. SEPARATION AND IMPROVEMENT IN DETECTION OF POLYCYCLIC AROMATIC HYDROCARBONS BY REVERSE-PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHY USING MICELLAR MOBILE PHASE AND FLUORESCENCE DETECTOR [J] . Hadjmohammadi MR, Fatemi MH Journal of Liquid Chromatography . 1995,第13期

机译：反相液相色谱-荧光检测器反相高效液相色谱法检测和分离多环芳烃
2. Micellar liquid chromatography of polycyclic aromatic hydrocarbons: Alkylpyridinium chloride as mobile phase modifier and selective fluorescence quencher [J] . Chunfeng Mao, Kelly E. McGill, Sheryl A. Tucker Journal of separation science. . 2003,第18期

机译：多环芳烃的胶束液相色谱：氯化烷基吡啶作为流动相改性剂和选择性荧光猝灭剂
3. SEPARATION OF POLYCYCLIC AROMATIC HYDROCARBONS BY MICELLAR ELECTROKINETIC CHROMATOGRAPHY WITH LASER FLUORESCENCE DETECTION [J] . Kaneta T., Imasaka T., Yamashita T. Analytica chimica acta . 1995,第3期

机译：胶束电动色谱-激光荧光检测法分离多环芳烃
4. Etched Stainless Steel Powder as Novel Sorbent Material for Solid-phase Extraction Coupled with High-performance Liquid Chromatography for Determination of Polycyclic Aromatic Hydrocarbons in Water [C] . Xiao YANG, Bao-Hui LI International Conference on Mechatronics Engineering and Modern Technologies in Industrial Engineering . 2015

机译：蚀刻不锈钢粉作为用于固相萃取的新型吸附剂材料与高性能液相色谱相结合，用于测定水中多环芳烃
5. The analysis of particulate and vapor phase polycyclic aromatic hydrocarbons in atmospheric samples using liquid chromatography with fluorescence detection and gas chromotography with mass spectrometric detection [D] . Duggan, Kathleen P. 2001

机译：液相色谱-荧光检测和气相色谱-质谱法分析大气样品中的颗粒和气相多环芳烃
6. Determination of polycyclic aromatic hydrocarbons with molecular mass 302 in Standard Reference Material 1597a by reversed-phase liquid chromatography and stop-flow fluorescence detection [O] . Hugh V. Hayes, Walter B. Wilson, Lane C. Sander, -1

机译：反相液相色谱和停流荧光检测法测定标准参考物质1597a中分子量为302的多环芳烃
7. A Novel Protocol to Monitor Trace Levels of Selected Polycyclic Aromatic Hydrocarbons in Environmental Water Using Fabric Phase Sorptive Extraction Followed by High Performance Liquid Chromatography-Fluorescence Detection [O] . Shivender Saini, Abuzar Kabir, Avasarala Rao, 2017

机译：一种新的方案，用于使用织物相吸附萃取在环境水中监测所选多环芳烃烃的痕量水平，其高效液相色谱 - 荧光检测
8. Applications of electrochemically-modulated liquid chromatography (EMLC): Separations of aromatic amino acids and polycyclic aromatic hydrocarbons [R] . Deng, L. 1998

机译：电化学调制液相色谱（EmLC）的应用：芳香族氨基酸和多环芳烃的分离

SEPARATION AND IMPROVEMENT IN DETECTION OF POLYCYCLIC AROMATIC HYDROCARBONS BY REVERSE-PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHY USING MICELLAR MOBILE PHASE AND FLUORESCENCE DETECTOR

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