Inductively coupled plasma atomic emission determination of impurities in high-purity niobium and tantalum oxides after separation of the matrix on a Polyorgs VII sorbent

O. N. Grebneva; N. I. Shchetinina; I. V. Kubrakova

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Inductively coupled plasma atomic emission determination of impurities in high-purity niobium and tantalum oxides after separation of the matrix on a Polyorgs VII sorbent

机译：在Polyorgs VII吸附剂上分离基质后，电感耦合等离子体原子发射光谱法测定高纯度铌和钽氧化物中的杂质

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Two methods were suggested for determining impurities in niobium and tantalum matrices: determination by inductively coupled plasma atomic emission spectrometry (ICP-AES) without preconcentration and determination alter sorption separation of the matrix. Spectral interferences in the ICP-AES determination of impurities m the above matrices were examined. Interelement correction factors were calculated, and sorption behavior of niobium, tantalum, and some other elements on a Polyorgs VII sorbent was studied. From this study, conditions for sorption separation of the matrices were chosen. In addition, procedures for the ICP-AES determination of impurities in high-purity niobium and tantalum oxides were developed (the determination limits are n X 10-0.n #mu#g/g).

机译：提出了两种测定铌和钽基质中杂质的方法：通过电感耦合等离子体原子发射光谱法（ICP-AES）进行测定而不进行预浓缩，以及测定改变基质的吸附分离度的方法。检查了上述基质中ICP-AES中杂质的光谱干扰。计算了元素校正因子，并研究了铌，钽和其他一些元素在Polyorgs VII吸附剂上的吸附行为。从这项研究中，选择了吸附分离基质的条件。另外，开发了ICP-AES测定高纯铌和钽氧化物中杂质的方法（测定极限为n X 10-0.n＃mu＃g / g）。

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《Журнал аналитической химии》 |1998年第1期|共6页
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O. N. Grebneva; N. I. Shchetinina; I. V. Kubrakova;
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1. Inductively coupled plasma atomic emission determination of impurities in high-purity niobium and tantalum oxides after separation of the matrix on a Polyorgs VII sorbent [J] . O. N. Grebneva, N. I. Shchetinina, I. V. Kubrakova Журнал аналитической химии . 1998,第1期

机译：在Polyorgs VII吸附剂上分离基质后，电感耦合等离子体原子发射光谱法测定高纯度铌和钽氧化物中的杂质
2. Determination of Impurities in Vanadium Disilicide and Vanadium Pentoxide by Atomic Absorption Spectrometry and Inductively Coupled Plasma-Atomic Emission Spectrometry after Matrix Separation [J] . Muneyuki KOHRI, Osamu KUJIRAI, Haruno OKOCHI Analytical Sciences . 1991,第5期

机译：原子吸收光谱法-电感耦合等离子体原子发射光谱法测定二硅化钒和五氧化二钒中的杂质
3. DIRECT DETERMINATION OF TRACE ELEMENTS IN NIOBIUM, TANTALUM AND THEIR OXIDES BY INDUCTIVELY COUPLED PLASMA ATOMIC EMISSION SPECTROMETRY AFTER MICROWAVE DISSOLUTION [J] . Grebneva ON., Kudinova TF., Kuzmin NM., Spectrochimica Acta, Part B. Atomic Spectroscopy . 1997,第8期

机译：微波溶解后电感耦合等离子体原子发射光谱法直接测定铌，钽及其氧化物中的微量元素。
4. Determination of tantalum and trace lanthanum, yttriumin superalloys by inductively coupled plasma atomic-emission spectrometry [C] . WangRong International conference on engineering and technological sciences;ICETS2000 . 2000

机译：电感耦合等离子体原子发射光谱法测定钽和痕量镧钇钇超合金
5. Studies of an end-on inductively coupled plasma atomic emission spectrometer (ICP-AES) and a direct sample insertion inductively coupled plasma atomic emission spectrometer (DSI-ICP-AES). [D] . Chen, Guangcheng. 1999

机译：末端感应电感耦合等离子体原子发射光谱仪（ICP-AES）和直接样品插入电感耦合等离子体原子发射光谱仪（DSI-ICP-AES）的研究。
6. Efficacy of engineered GO Amberlite XAD-16 picolylamine sorbent for the trace determination of Pb (II) and Cu (II) in fishes by solid phase extraction column coupled with inductively coupled plasma optical emission spectrometry [O] . Hina Javed, Aminul Islam, Anjali Chauhan, -1

机译：固相萃取柱-电感耦合等离子体发射光谱法测定工程GO Amberlite XAD-16甲基吡啶胺吸附剂痕量测定鱼类中的Pb（II）和Cu（II）的功效
7. Determination of Ultra-trace Metal Impurities in High-purity Cadmium Using Inductively Coupled Plasma Mass Spectrometry after Matrix Separation with Anion Exchange Resin [O] . Ayaka WADA, Naoko NONOSE, Masaki OHATA, 2017

机译：用阴离子分离后使用电感耦合等离子体质谱法测定高纯度镉中的超痕量金属杂质
8. Determination of Impurities in Silicon Carbide by ICP AES (Inductively Coupled Plasma Atomic Emission Spectrometry) after Coprecipitation with Lanthanum Hydroxide [R] . Harada, Y., Kurata, N., Furuno, G. 1988

机译：氢氧化镧共沉淀ICp-aEs（电感耦合等离子体原子发射光谱法）测定碳化硅中的杂质

Inductively coupled plasma atomic emission determination of impurities in high-purity niobium and tantalum oxides after separation of the matrix on a Polyorgs VII sorbent

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