Direct sample injection into an open tubular column of large diameter without flow splitting

I. N. Stankov; S. N. Tarasov

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Direct sample injection into an open tubular column of large diameter without flow splitting

机译：将样品直接注射到大直径的开放式管状色谱柱中，而不会发生分流

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摘要

Some parameters of direct sample injection into an open tubular column of large diameter without flow splitting (volume of the injected sample, temperature of the injection port, flow rate of the carrier gas, and the completeness of sample transfer) were studied. Optimal operating conditions of an injection port were determined; it was demonstrated that this technique of sample injection can be used for the analysis of mixtures of compounds of different classes.

机译：研究了将样品直接注射到大直径开口管柱中而没有分流的一些参数（注射样品的体积，注射端口的温度，载气的流速和样品转移的完整性）。确定了进样口的最佳运行条件;事实证明，这种进样技术可用于分析不同类别化合物的混合物。

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《Журнал аналитической химии》 |1999年第11期|共6页
作者
I. N. Stankov; S. N. Tarasov;
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原文格式 PDF
正文语种 rus
中图分类分析化学;
关键词
direct sample injection; open tubular column; flow splitting;

机译：直接进样;开放管柱;分流;

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专利

1. Direct sample injection into an open tubular column of large diameter without flow splitting [J] . I. N. Stankov, S. N. Tarasov Журнал аналитической химии . 1999,第11期

机译：将样品直接注射到大直径的开放式管状色谱柱中，而不会发生分流
2. SEPARATION AND QUANTIFICATION OF COMPONENTS OF EDIBLE FAT UTILIZING OPEN TUBULAR COLUMNS IN SFC - SAMPLE INTRODUCTION BY DIRECT INJECTION AND SFE COUPLED ON-LINE TO SFC [J] . Berg BE., Greibrokk T., Lund HS. Chromatographia . 1997,第7a8期

机译：在SFC中使用露天管柱的可食用脂肪组分的分离和定量 - 样品介绍直接注射和SFE在线到SFC
3. Curtain flow chromatography ('the infinite diameter column') with automated injection and high sample through-put: The results of an inter-laboratory study [J] . Foley D., Pereira L., Camenzuli M., Microchemical Journal: Devoted to the Application of Microtechniques in all Branches of Science . 2013,第Null期

机译：自动进样和高样品通量的幕流色谱（“无限直径色谱柱”）：实验室间研究的结果
4. Zeptomole Level Proteomic Analysis of Limited Availability Clinical Samples Using Monolithic and Porous Layer Open Tubular Columns in Ultralow Flow LC/MS [C] . Alexander R. Ivanov, Siyang Li, Simion Kreimer, American Society for Mass Spectrometry Conference on Mass Spectrometry and Allied Topics . 2013

机译：Zeptomole水平使用超级流动LC / MS中的单片和多孔层张开管柱的限量可用性临床样品的蛋白质组学分析
5. Investigating unsaturated flow for heap leach materials in large diameter columns. [D] . Galla, Vivek. 2007

机译：研究大直径塔中堆浸物料的不饱和流量。
6. Flow Rate Concentration and Saturation: Investigating the Fundamentals of Sample-Trapped Column Injection [O] . H. Svobodova, A. Berg, G. Valaskovic, 2011

机译：流速浓度和饱和度：研究样品阱色谱柱进样的基本原理
7. ELUENT CONDITIONS FOR DIRECT INJECTIONS OF INTACT PLASMA SAMPLES ONTO A DUAL MODE COLUMN [O] . SHINOBU KUDOH, HIROSHI NAKAMUBA 1991

机译：用于将完整的等离子体样品直接注射到双模柱上的洗脱条件
8. Comparison of continuous pneumatic nebulization and flow injection-direction injection nebulization for sample introduction in inductively coupled plasma-mass spectrometry [R] . Crain, J. S. , Kiely, J. T. 1997

机译：连续气动雾化和流动注射方向注射雾化在电感耦合等离子体质谱中引入样品的比较

Direct sample injection into an open tubular column of large diameter without flow splitting

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