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Design and Fabrication of a Furnace for High-Temperature Neutron Powder Diffraction Measurements, and Structural Study of Ceramic Materials

机译:高温中子粉末衍射测量炉的设计与制造以及陶瓷材料的结构研究

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摘要

We have designed and fabricated a new furnace for high-temperature neutron-diffraction measurements. The furnace does not yield any extra peaks due to heaters and refractory, thus we were able to measure very small neutron signals from the sample. Quality neutron diffraction data at high temperatures up to about 1590 deg C were analyzed by Rietveld method for various materials as zirconia and calcium titanate.
机译:我们设计和制造了一种用于高温中子衍射测量的新型熔炉。由于加热器和耐火材料,熔炉不会产生任何额外的峰值,因此我们能够测量样品中非常小的中子信号。通过Rietveld方法分析了氧化锆和钛酸钙等各种材料在高达约1590摄氏度的高温下的优质中子衍射数据。

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