Mild and efficient protection of diol and carbonyls as cyclic acetals catalysed by iron (III) chloride

Iyad Karame; Mohamad Alame; Ali Kanj

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Mild and efficient protection of diol and carbonyls as cyclic acetals catalysed by iron (III) chloride

机译：氯化铁（III）催化温和有效地保护二醇和羰基化合物作为环状缩醛

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摘要

A friendly method for the protection of diols and carbonyls catalysed by hexahydrated iron (III) chloride has been developed. This method, which consists of the transformation of diols and carbonyls to cyclic acetals, functions in mild conditions and it is efficient for a wide range of diols.

机译：已经开发出保护六水合氯化铁（III）催化的二醇和羰基的友好方法。该方法由二醇和羰基化合物向环状缩醛的转化组成，在温和的条件下起作用，对多种二醇都有效。

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《Comptes Rendus Chimie》 |2011年第6期|共5页
作者
Iyad Karame; Mohamad Alame; Ali Kanj;
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原文格式 PDF
正文语种 eng
中图分类化学;
关键词
Cyclic acetal; Diol; Carbonyl; Iron; Protection;

机译：环缩醛;二醇;羰基;铁;保护;

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专利

1. Mild and efficient protection of diol and carbonyls as cyclic acetals catalysed by iron (III) chloride [J] . Iyad Karame, Mohamad Alame, Ali Kanj Comptes Rendus Chimie . 2011,第6期

机译：氯化铁（III）催化温和有效地保护二醇和羰基化合物作为环状缩醛
2. A Simple, Efficient and General Procedure for Acetalization of Carbonyl Compounds and Deprotection of Acetals under the Catalysis of Indium(III) Chloride [J] . Brindaban C. Ranu, Ranjan Jana Advanced synthesis & catalysis . 2004,第4期

机译：氯化铟（III）催化下羰基化合物的缩醛化和缩醛缩醛的简单，高效，通用程序
3. Bis (salicylaldehyde-1, 2-phenylene diimine)Mn(III) chloride (Mn(III)-salophen) catalysed oxidation of thiols to symmetrical disulfides using urea hydrogen peroxide (UHP) as mild and efficient oxidant [J] . Karami B, Montazerozohori M, Habibi MH Journal of Chemical Research. Synopses . 2006,第8期

机译：使用过氧化氢脲（UHP）作为温和有效的氧化剂，双（水杨醛-1，2-亚苯基二亚胺）氯化氯化锰（III）-卤化苯酚将硫醇氧化为对称的二硫化物。
4. Iron(III) chloride : an efficient catalyst for the regioselective protection of saccharides [C] . Yann Bourdreux, Aurelie Lemetais, Dominique Urban European Symposium on Organic Chemistry . 2009

机译：铁（III）氯化物：糖类区域的有效催化剂
5. Behavior of gold (III) chloride during the precipitation of iron (III)/arsenic (V) in aqueous media under atmospheric and pressure conditions [D] . Blais, Derek 2011

机译：大气和压力条件下，水性介质中铁（III）/砷（V）沉淀过程中氯化金（III）的行为
6. Peripheral mechanism of a carbonyl hydrosilylation catalysed by an SiNSi iron pincer complex [O] . Toni T. Metsänen, Daniel Gallego, Tibor Szilvási, 2015

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7. Phenolic acetals from lignins of varying compositions via iron(III) triflate catalysed depolymerisation [O] . Deuss, Peter J., Lancefield, Christopher S., Narani, Anand, 2017

机译：通过三氟甲磺酸铁（III）催化不同组成的木质素的酚醛缩醛

Mild and efficient protection of diol and carbonyls as cyclic acetals catalysed by iron (III) chloride

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