Slurry explosive detonation synthesis and characterization of 10 nm TiO2

Yan Honghao; Zhao Tiejun; Li Xiaojie; Zhao Bibo

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Slurry explosive detonation synthesis and characterization of 10 nm TiO2

机译：浆料炸药爆轰的合成与表征10 nm TiO2

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TiO2 was prepared by detonating a slurry explosive made of Ti precursor, ammonium nitrate, cyclo-trimethylenetrinitramine (RDX), and polystyrene (EPS). X-ray diffraction, transmission electron microscopy, energy dispersive X-ray spectrometry, Fourier transform infrared spectroscopy, and UV vis diffuse reflection spectroscopy revealed that the sample was composed of mixed crystals of rutile and anatase TiO2 with irregular spherical shapes and 10 nm particle size. The minimum energy gap of the sample was 2.9 eV. An ideal TiO2 explosive was prepared from a precursor/ammonium nitrate/RDX ratio of 1:1:0.6 and 2 g of EPS as a density modifier. (C) 2016 Elsevier Ltd and Techna Group S.r.l. All rights reserved.

机译：通过引爆由Ti前驱物，硝酸铵，环三亚甲基三硝胺（RDX）和聚苯乙烯（EPS）制成的浆料炸药来制备TiO2。 X射线衍射，透射电子显微镜，能量色散X射线光谱，傅立叶变换红外光谱和UV可见漫反射光谱显示样品由金红石和锐钛矿型TiO2混合晶体组成，球形不规则，粒径为10 nm。。样品的最小能隙为2.9 eV。理想的TiO2炸药是由前体/硝酸铵/ RDX比例为1：1：0.6和2 g EPS作为密度调节剂制备的。（C）2016 Elsevier Ltd和Techna Group S.r.l.版权所有。

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《CERAMICS INTERNATIONAL》 |2016年第13期|共5页
作者
Yan Honghao; Zhao Tiejun; Li Xiaojie; Zhao Bibo;
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正文语种 eng
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10 nm; Slurry explosive; TiO2;

机译：10 nm;浆状炸药;TiO2;

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Slurry explosive detonation synthesis and characterization of 10 nm TiO2

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