Rhodium(III)-catalyzed amidation of aryl ketone o-methyl oximes with isocyanates by C-H activation: Convergent synthesis of 3-methyleneisoindolin-1- ones

Zhou B.; Hou W.; Yang Y.; Li Y.

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Rhodium(III)-catalyzed amidation of aryl ketone o-methyl oximes with isocyanates by C-H activation: Convergent synthesis of 3-methyleneisoindolin-1- ones

机译：铑（III）的C-H活化催化芳基酮邻甲基肟与异氰酸酯的酰胺化反应：3-亚甲基异吲哚啉-1的聚合合成

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Going green! The rhodium(III)-catalyzed annulation of aryl ketone O-methyl oximes with isocyanates for the synthesis of 3-methyleneisoindolin-1-ones is reported (see scheme). This reaction exhibits high regioselectivity, functional-group tolerance, and broad substrate scope, without the use of additives or production of environmentally hazardous waste.

机译：走向绿色！据报道，铑（III）催化的芳基酮O-甲基肟与异氰酸酯的环合反应可合成3-亚甲基异吲哚啉-1-酮（参见方案）。该反应显示出高区域选择性，官能团耐受性和广泛的底物范围，而无需使用添加剂或不产生对环境有害的废物。

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《Chemistry: A European journal》 |2013年第15期|共6页
作者
Zhou B.; Hou W.; Yang Y.; Li Y.;
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正文语种 eng
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关键词
annulation; C-H activation; isocyanates; ketones; rhodium;

机译：环化;C-H活化;异氰酸酯;酮;铑;

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1. Rhodium(III)-catalyzed amidation of aryl ketone o-methyl oximes with isocyanates by C-H activation: Convergent synthesis of 3-methyleneisoindolin-1- ones [J] . Zhou B., Hou W., Yang Y., Chemistry: A European journal . 2013,第15期

机译：铑（III）的C-H活化催化芳基酮邻甲基肟与异氰酸酯的酰胺化反应：3-亚甲基异吲哚啉-1的聚合合成
2. Regioselective Synthesis of Indenols by Rhodium-Catalyzed C-H Activation and Carboeyclization of Aryl Ketones and Alkynes [J] . Krishnamoorthy Muralirajan, Kanniyappan Parthasarathy, Chien-Hong Cheng Angewandte Chemie . 2011,第18期

机译：铑催化的C-H活化和芳基酮和炔烃的羰基化反应区域选择性合成茚基
3. Regioselective Synthesis of Indenols by Rhodium-Catalyzed C-H Activation and Carboeyclization of Aryl Ketones and Alkynes [J] . Krishnamoorthy Muralirajan, Kanniyappan Parthasarathy, Chien-Hong Cheng Angewandte Chemie . 2011,第18期

机译：铑催化的C-H活化和芳基酮和炔烃的羰基化反应区域选择性合成茚基
4. Rhodium(III)-Catalyzed Direct C-H Bond Amidation of AnilineDerivatives Using a Pyrimidyl Directing Group [C] . Shrikant M.Khake, Naoto Chatani 日本化学会春季年会 . 2020

机译：使用嘧啶指针组 - 催化（III） - 催化直接C-H键合粘合剂酰胺
5. Part I. Asymmetric hydrosilylation of acetophenone using titanium catalysts. Part II. Synthesis of water-soluble palladacycles and their applications to the Suzuki reaction. Part III. Rhodium-catalyzed addition of aryl and alkenylboronic acids to aldehyde [D] . Huang, Rongcai. 2005

机译：第一部分：使用钛催化剂的苯乙酮不对称氢化硅烷化。第二部分水溶性palladacycles的合成及其在铃木反应中的应用。第三部分铑催化的芳基和烯基硼酸加成醛
6. Rhodium(III)-Catalyzed Alkenyl C-H Bond Functionalization for the Convergent Synthesis of Furans and Pyrroles [O] . Yajing Lian, Tatjana Huber, Kevin D. Hesp, -1

机译：铑（III） - 催化链烯基C-H键官能化用于呋喃和胃肠杆菌的收敛合成
7. Rhodium(III)-Catalyzed C-H Activation and Amidation of Arenes Using N-Arenesulfonated Imides as Amidating Reagents [O] . Yu Songjie, Wan Boshun, Li Xingwei 2013

机译：Rhodium(III)-Catalyzed C-H activation and amidation of arenes Using N-arenesulfonated Imides as amidating Reagents

Rhodium(III)-catalyzed amidation of aryl ketone o-methyl oximes with isocyanates by C-H activation: Convergent synthesis of 3-methyleneisoindolin-1- ones

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