Determination of Amino Acid Enantiopurity and Absolute Configuration: Synergism between Configurationally Labile Metal-Based Receptors and Dynamic Covalent Interactions

Francesca A. Scaramuzzo; Giulia Licini; Cristiano Zonta

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Determination of Amino Acid Enantiopurity and Absolute Configuration: Synergism between Configurationally Labile Metal-Based Receptors and Dynamic Covalent Interactions

机译：氨基酸对映体纯度和绝对构型的确定：不稳定金属基受体与动态共价相互作用的协同作用

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Reliable determination of the enantiomeric excess of free amino acids can be obtained by measuring the induced circular dichroism of a multicomponent assembly formed by a modified tris(2-pyridylmethyl)amine ligand, a zinc salt, and the amino acid of interest. The systems furnish reliable information for all natural amino acids.

机译：通过测量由修饰的三（2-吡啶甲基甲基）胺配体，锌盐和目标氨基酸形成的多组分组件的诱导圆二色性，可以可靠地确定游离氨基酸的对映体过量。该系统可为所有天然氨基酸提供可靠的信息。

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《Chemistry: A European journal》 |2013年第49期|共5页
作者
Francesca A. Scaramuzzo; Giulia Licini; Cristiano Zonta;
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正文语种 eng
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amino acids; configuration determination; circular dichroism; chirality; ligands; molecular recognition;

机译：氨基酸;构型测定;圆二色性;手性;配体;分子识别;

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1. Determination of Amino Acid Enantiopurity and Absolute Configuration: Synergism between Configurationally Labile Metal-Based Receptors and Dynamic Covalent Interactions [J] . Francesca A. Scaramuzzo, Giulia Licini, Cristiano Zonta Chemistry: A European journal . 2013,第49期

机译：氨基酸对映体纯度和绝对构型的确定：不稳定金属基受体与动态共价相互作用的协同作用
2. A simple ternary ion-pair complexation protocol for testing the enantiopurity and the absolute configurational analysis of acid and ester derivatives [J] . Arya Neeru, Mishra Sandeep Kumar, Suryaprakash N. New Journal of Chemistry . 2018,第12期

机译：一种简单的三元离子对络合方案，用于测试对酸和酯衍生物的对映储荷和绝对配置分析
3. A new method proposed for the determination of absolute configurations of alpha-amino acids [J] . Gomez ED, Duddeck H Magnetic Resonance in Chemistry: MRC . 2009,第3期

机译：一种新的测定α-氨基酸绝对构型的方法
4. The "Bip Method" for Spectroscopic Assignment of the Absolute Configuration of the Spin-Labelled, Cyclic β~(2,6)-Amino Acids β-TOAC and POAC [C] . Karen Wright, Laurence Dutot, Anne Gaucher American Peptide Symposium . 2009

机译：用于光谱分配的“BIP方法”，用于旋转标记的循环β〜（2,6） - 氨基酸β-TOAC和POAC的绝对构型
5. Determination of the Absolute Configuration of β-Chiral Primary Alcohols Using the Competing Enantioselective Conversion Method Heteroatom-directed Acylation of Secondary Alcohols to Assign Absolute Configuration Total Synthesis of Illisimonin a Osmate Es [D] . Burns, Alexander Sunshine. 2020

机译：使用竞争对映选择性转化法测定β-chiral初级醇的绝对构型次原子为仲醇的酰化酰化，分配绝对构型Illisimonin的总合成渗透
6. Absolute configuration retention of a configurationally labile ligand during dynamic processes of thiolate protected gold clusters [O] . Yanan Wang, Esko Makkonen, Xi Chen, 2021

机译：硫醇酸盐保护金簇动态过程中的配置不稳定的绝对配置保留
7. Studies on Optically Active Amino Acids. VIII. Studies on α-Alkyl-α-amino Acids. III. Determination of Absolute Configuration of Optically Active Isovaline. [O] . Kazuo Achiwa, Shun-ichi Yamada 1966

机译：对光学活性氨基酸的研究。 VIII。研究α-烷基-α-氨基酸。 III。光学活性依伐的绝对结构的测定。

Determination of Amino Acid Enantiopurity and Absolute Configuration: Synergism between Configurationally Labile Metal-Based Receptors and Dynamic Covalent Interactions

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