Transition-metal-free one-pot synthesis of biaryls from grignard reagents and substituted cyclohexanones

Zhou F.; Simon M.-O.; Li C.-J.

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Transition-metal-free one-pot synthesis of biaryls from grignard reagents and substituted cyclohexanones

机译：格氏试剂和取代的环己酮的无过渡金属一锅法合成联芳基

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摘要

A new strategy for the construction of biaryls by a transition-metal-free process is presented. A sequence of a Grignard reaction, dehydration, and oxidative aromatization affords the desired products in a one-pot fashion.

机译：提出了一种通过无过渡金属工艺制备联芳基的新策略。格氏反应，脱水和氧化芳构化的一系列步骤以一锅方式提供所需的产品。

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《Chemistry: A European journal》 |2013年第22期|共5页
作者
Zhou F.; Simon M.-O.; Li C.-J.;
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正文语种 eng
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关键词
biaryls; cyclohexanone; Grignard reaction; one-pot process; transition-metal free;

机译：联芳基;环己酮;格氏反应;一锅法;无过渡金属;

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专利

1. Transition-metal-free one-pot synthesis of biaryls from grignard reagents and substituted cyclohexanones [J] . Zhou F., Simon M.-O., Li C.-J. Chemistry: A European journal . 2013,第22期

机译：格氏试剂和取代的环己酮的无过渡金属一锅法合成联芳基
2. A one-pot synthesis of 1-substituted cyclic phosphine sulfides by simultaneous addition of bis- and mono-grignard reagents to a new efficient phosphorus donating reagent [J] . Baccolini G., Negri U., Boga C. Synlett . 2000,第11期

机译：通过将双格氏试剂和单格氏试剂同时添加到新型高效供磷试剂中，一锅法合成1-取代的环膦硫化物
3. [Pd(μ-Cl)Cl(IPr~*)]_2: a highly hindered pre-catalyst for the synthesis of tetra-ortho-substituted biaryls via Grignard reagent cross-coupling [J] . Mathieu Lesieur, Alexandra M. Z. Slawin, Catherine S. J. Cazin Organic & biomolecular chemistry . 2014,第30期

机译：[Pd（μ-Cl）Cl（IPr〜*）] _ 2：格氏试剂交叉偶联合成四邻位取代联芳基的高度受阻前催化剂
4. gamma-Selective Allylic Substitution Reaction with Grignard Reagents Catalyzed by Copper N-Heterocyclic Carbene Complexes [C] . Sentaro Okamoto, Satoshi Tominaga, Yukinao Oi, Symposium on Organometallic Chemistry . 2004

机译：γ-选择性烯丙基取代反应与铜正杂环碳络合物催化的格氏试剂
5. Porphyrins: A solvent free synthesis, combinatorial libraries, a solid phase synthesis, and towards a tetra-Grignard reagent. [D] . Gong, Xianchang. 2000

机译：卟啉：无溶剂合成，组合库，固相合成和四格氏试剂。
6. One-pot synthesis of meso-alkyl substituted isocorroles: the reaction of a triarylcorrole with Grignard reagent [O] . Sara Nardis, Giuseppe Pomarico, Federica Mandoj, -1

机译：单罐合成中烷基取代的异漏剂：三芳咯尔与格氏试剂的反应
7. One-pot synthesis of meso-alkyl substituted isocorroles: The reaction of a triarylcorrole with Grignard reagent [O] . Nardis, S, Pomarico, G, Mandoj, F, 2010

机译：一锅法合成中烷基取代的异Corroles：三芳基Corrole与Grignard试剂的反应

Transition-metal-free one-pot synthesis of biaryls from grignard reagents and substituted cyclohexanones

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