Efficient Synthesis of Eight-Membered Nitrogen Heterocycles from O-Propargylic Oximes by Rhodium-Catalyzed Cascade Reactions

Itaru Nakamura; Yoshinori Sato; Keisuke Takeda; Masahiro Terada

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Efficient Synthesis of Eight-Membered Nitrogen Heterocycles from O-Propargylic Oximes by Rhodium-Catalyzed Cascade Reactions

机译：铑催化级联反应从邻丙炔肟高效合成八元氮杂环

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摘要

Azocine derivatives were successfully synthesized from O-propargylic oximes by means of a Rh-catalyzed 2,3-rearrangement/heterocyclization cascade reaction. Moreover, the chirality of the substrate was maintained throughout the cascade process to afford the corresponding optically active azocines.

机译：通过Rh催化的2，3-重排/杂环级联反应，成功地从O-炔丙基肟合成了偶氮衍生物。此外，在整个级联过程中维持底物的手性，以提供相应的光学活性偶氮碱。

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《Chemistry: A European journal》 |2014年第33期|共6页
作者
Itaru Nakamura; Yoshinori Sato; Keisuke Takeda; Masahiro Terada;
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正文语种 eng
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Azocine; derivatives; successfully;

机译：偶氮素;衍生物;成功;

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1. Efficient Synthesis of Eight-Membered Nitrogen Heterocycles from O-Propargylic Oximes by Rhodium-Catalyzed Cascade Reactions [J] . Itaru Nakamura, Yoshinori Sato, Keisuke Takeda, Chemistry: A European journal . 2014,第33期

机译：铑催化级联反应从邻丙炔肟高效合成八元氮杂环
2. Oxazepine Synthesis by Copper-Catalyzed Intermolecular Cascade Reactions between O-Propargylic Oximes and Dipolarophiles [J] . Itaru Nakamura, Masahiro Terada, Yu Kudo Angewandte Chemie . 2013,第29期

机译：O-炔丙基肟与双极性亲核剂之间的铜催化分子间级联反应合成奥氮平
3. Rhodium-Catalyzed Sequential Allylic Animation and Olefin Hydroacylation Reactions: Enantioselective Synthesis of Seven-Membered Nitrogen Heterocycles [J] . Jeffrey S. Arnold, Edward T. Mwenda, Hien M. Nguyen Angewandte Chemie . 2014,第14期

机译：铑催化的顺序烯丙基动画和烯烃加氢酰化反应：七元氮杂环的对映选择性合成。
4. Synthesis of Nitrogen Heterocycles though Rhodium-Catalyzed 2+2+2 Cycloaddition [C] . Azusa Wada, Nanami Suzuki, Ken Tanaka Symposium on Organometallic Chemistry . 2006

机译：氮杂环的合成虽然铑催化2 + 2 + 2环加成
5. Enantioselective synthesis of substituted polycyclic heterocycles by rhodium-catalyzed ring-opening reactions of aryne Diels-Alder adducts [D] . Nguyen, Duc Trung. 2009

机译：芳烃Diels-Alder加合物的铑催化开环反应对映选择性合成多环杂环
6. Synthesis of Polycyclic Nitrogen Heterocycles via Cascade Pd-Catalyzed Alkene Carboamination/Diels-Alder Reactions [O] . Derick R. White, John P. Wolfe -1

机译：级联钯催化的烯烃碳氨基化/ Diels-Alder反应合成多环氮杂环
7. Design and synthesis of a novel class of CK2 inhibitors: application of copper- and gold-catalysed cascade reactions for fused nitrogen heterocycles. [O] . Suzuki Yamato, Oishi Shinya, Takei Yoshinori, 2012

机译：一类新型CK2抑制剂的设计和合成：铜和金催化的级联反应用于稠合氮杂环的应用。

Efficient Synthesis of Eight-Membered Nitrogen Heterocycles from O-Propargylic Oximes by Rhodium-Catalyzed Cascade Reactions

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