Dynamic Formation of Noncovalent Calixsalen Aggregates

Petryk Malgorzata; Troc Anna; Gierczyk Blazej; Danikiewicz Witold; Kwit Marcin

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Dynamic Formation of Noncovalent Calixsalen Aggregates

机译：动态形成非共价杯形聚集物

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A procedure for studying dynamic structural behavior of large chiral macrocycles is presented. Ion mobility MS, diffusion-ordered NMR spectroscopy (DOSY NMR), and optical rotation (OR) measurements, supported by calculations, are used together as effective complementary methods to study dynamic formation of noncovalent aggregates. It is shown that the monomer-dimer equilibrium is driven by - or CH- interactions and controlled largely by the substitution pattern of the calixsalen skeleton.

机译：提出了研究大型手性大环动力学结构行为的程序。离子迁移率MS，扩散有序NMR光谱（DOSY NMR）和旋光性（OR）测量（受计算支持）一起用作研究非共价聚集体动态形成的有效补充方法。结果表明，单体-二聚体平衡是由-或CH-相互作用驱动的，并且在很大程度上受杯盖素骨架的取代方式控制。

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《Chemistry: A European journal》 |2015年第29期|共4页
作者
Petryk Malgorzata; Troc Anna; Gierczyk Blazej; Danikiewicz Witold; Kwit Marcin;
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正文语种 eng
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关键词
calixsalens; ion mobility MS; NMR; optical rotation; self-assembly;

机译：杯芳烃;离子迁移率MS;NMR;旋光性;自组装;

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专利

1. Dynamic Formation of Noncovalent Calixsalen Aggregates [J] . Petryk Malgorzata, Troc Anna, Gierczyk Blazej, Chemistry: A European journal . 2015,第29期

机译：动态形成非共价杯形聚集物
2. Conformational Transformations in Chiral Polythiophene Derivatives Aggregated in Polymethacrylate Matrices: Experiments and Molecular Dynamics Simulations [J] . Thomas Bjornholm, Witold Brostow, Kjeld Schaumburg, Macromolecular symposia . 1999,第0期

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3. Unexpected formation of a tubular architecture by optically active pure organic calixsalen [J] . Petryk Malgorzata, Janiak Agnieszka, Kwit Marcin CrystEngComm . 2017,第39期

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Dynamic Formation of Noncovalent Calixsalen Aggregates

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