A Fast Way to Fluorescence: A Fourfold Domino Reaction to Condensed Polycyclic Compounds

Lutz F. Tietze; Christoph Eichhorst; Tim Hungerland; Markus Steinert

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A Fast Way to Fluorescence: A Fourfold Domino Reaction to Condensed Polycyclic Compounds

机译：荧光的快速方法：缩合多环化合物的四重多米诺反应

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A fast and efficient palladium-catalyzed fourfold domino Sonogashira/double-carbopalladation/C-H-activation reaction that converts simple aromatic systems into complex polycyclic hydrocarbons has been developed. A number of substituted products has thus been prepared in yields up to 89 %. The structural assignment has been confirmed by using single-crystal X-ray crystallography. The products show intriguing fluorescence activity and thus might serve as chemical sensors or fluorescent imaging dyes.

机译：已经开发了一种快速有效的钯催化四重多米诺Sonogashira /双羰基钯/ C-H活化反应，可将简单的芳族系统转化为复杂的多环烃。因此已经制备了许多取代的产物，产率高达89％。通过使用单晶X射线晶体学已经确认了结构分配。该产品显示出有趣的荧光活性，因此可以用作化学传感器或荧光成像染料。

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来源
《Chemistry: A European journal》 |2014年第39期|共6页
作者
Lutz F. Tietze; Christoph Eichhorst; Tim Hungerland; Markus Steinert;
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正文语种 eng
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关键词
C-H-activation; domino reactions; dyes/pigments; luminescence; palladium;

机译：C-H活化;多米诺反应;染料/色素;发光;钯;

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1. A Fast Way to Fluorescence: A Fourfold Domino Reaction to Condensed Polycyclic Compounds [J] . Lutz F. Tietze, Christoph Eichhorst, Tim Hungerland, Chemistry: A European journal . 2014,第39期

机译：荧光的快速方法：缩合多环化合物的四重多米诺反应
2. A New Multicomponent Domino Reaction of 1,3-Dicarbonyl Compounds:One-Pot Access to Polycyclic N/O-,N/S-,and N/N-Aminals [J] . Celine Simon, Jean-Francois Peyronel, Jean Rodriguez Organic letters . 2001,第14期

机译：1,3-二羰基化合物的新型多组分多米诺反应：一键接近多环N / O-，N / S-和N / N-胺
3. Study on fluorescence of Maillard reaction compounds in breakfast cereals [J] . Delgado-Andrade C, Rufian-Henares JA, Morales FJ Molecular Nutrition and Food Research . 2006,第9期

机译：早餐谷物中美拉德反应化合物的荧光研究
4. T- Jump/Time- of- Flight Mass Spectrometery for Time Resolved Analysis of Fast Condensed Stated Reactions [C] . L. Zhou, N. Piekiel, S. Chowdhury, AIAA Aerospace Sciences Meeting Including The New Horizons Forum and Aerospace Exposition . 2009

机译：T跳跃/飞行时间质谱用于快速凝聚态反应的时间分辨分析
5. Inverse electron demand Diels-Alder (IEDDA)-driven domino reactions of chromone-fused electron deficient dienes: New methodology for the synthesis of xanthones and xanthone-based polycyclic heteroaromatic molecules. [D] . Dang, Anh-Thu T. 2009

机译：逆电子需求Diels-Alder（IEDDA）驱动的色酮融合的电子缺陷二烯的多米诺反应：合成氧杂蒽酮和基于黄酮的多环杂芳族分子的新方法。
6. Preparation of neuroprotective condensed 14-benzoxazepines by regio- and diastereoselective domino Knoevenagel–15-hydride shift cyclization reaction [O] . László Tóth, Yan Fu, Hai Yan Zhang, 2014

机译：区域和非对映选择性多米诺Knoevenagel– 15-氢化物转移环化反应制备神经保护性缩合的14-苯并x庚因
7. Study on fluorescence of Maillard reaction compounds in breakfast cereals [O] . Delgado Andrade Cristina, Rufián Henares J. A., Morales F. J. 2014

机译：早餐谷物中美拉德反应化合物的荧光研究

A Fast Way to Fluorescence: A Fourfold Domino Reaction to Condensed Polycyclic Compounds

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