Fast and Efficient ~(18)F-Labeling by [~(18)F]Fluorophenylazocarboxylic Esters

Stefanie K. Fehler; Simone Maschauer; Sarah B. H?fling; Amelie L. Bartuschat; Nuska Tschammer; Harald Hübner; Peter Gmeiner; Olaf Prante; Markus R. Heinrich

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Fast and Efficient ~(18)F-Labeling by [~(18)F]Fluorophenylazocarboxylic Esters

机译：[〜（18）F]氟苯基偶氮羧酸酯的快速高效〜（18）F-标记

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Introduction of [~(18)F]fluoride ion into the aromatic core of phenylazocarboxylic esters was achieved in only 30 seconds, with radiochemical yields of up to 95% (85(±10) %). For labeling purposes, the resulting ~(18)F-substituted azoester can be further converted in radical-arylation reactions to give biaryls, or in substitutions at its carbonyl unit to produce azocarboxamides.

机译：仅在30秒内即可将[〜（18）F]氟离子引入苯偶氮羧酸酯的芳族核中，放射化学产率高达95％（85（±10）％）。为了标记的目的，可以将所得的〜（18）F-取代的偶氮酯在自由基芳基化反应中进一步转化成联芳基，或者在其羰基单元的取代基中生成偶氮羧酰胺。

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《Chemistry: A European journal》 |2014年第2期|共6页
作者
Stefanie K. Fehler; Simone Maschauer; Sarah B. H?fling; Amelie L. Bartuschat; Nuska Tschammer; Harald Hübner; Peter Gmeiner; Olaf Prante; Markus R. Heinrich;
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正文语种 eng
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phenylazocarboxylic; radiochemical; purposes;

机译：苯偶氮羧酸;放射化学;用途;

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1. Fast and Efficient ~(18)F-Labeling by [~(18)F]Fluorophenylazocarboxylic Esters [J] . Stefanie K. Fehler, Simone Maschauer, Sarah B. H?fling, Chemistry: A European journal . 2014,第2期

机译：[〜（18）F]氟苯基偶氮羧酸酯的快速高效〜（18）F-标记
2. Fast and efficient copper-mediated 18 F-fluorination of arylstannanes, aryl boronic acids, and aryl boronic esters without azeotropic drying [J] . Salla Orvokki Lahdenpohja, Noora Annika Rajala, Johan Rajander, EJNMMI Radiopharmacy and Chemistry . 2019,第1期

机译：快速高效的铜介导的18 F氟化芳基斯坦酮，芳基硼酸和芳基硼酸酯，无需共沸干燥
3. Alginate-Polymer-Caged, C_(18)-Functionalized Magnetic Titanate Nanotubes for Fast and Efficient Extraction of Phthalate Esters from Water Samples with Complex Matrix [J] . Hongyun Niu, Shengxiao Zhang, Xiaole Zhang ACS applied materials & interfaces . 2010,第4期

机译：海藻酸酯-聚合物笼，C_（18）-功能化的磁性钛酸盐纳米管，用于从复杂基质的水样品中快速高效地提取邻苯二甲酸酯。
4. Trypsin Immobilization on Hairy Polymer Chains Hybrid Magnetic Nanoparticles for Ultra Fast, Highly Efficient Proteome Digestion, Facile ~(18)O Labeling and Absolute Protein Quantification [C] . Weijie Qin, Zifeng Song, Yangjun Zhang, American Society for Mass Spectrometry Conference on Mass Spectrometry and Allied Topics . 2012

机译：胰蛋白酶固定在毛状聚合物链中杂交磁性纳米粒子用于超快速，高效的蛋白质组消化，容易〜（18）o标记和绝对蛋白质量化
5. ATM/ATR-mediated phosphorylation of RAD18 is required for efficient S-phase progression and replication fork stability. [D] . Gurkar, Aditi Uday. 2010

机译：有效的S期进程和复制叉稳定性需要ATM / ATR介导的RAD18磷酸化。
6. Fast and efficient copper-mediated 18F-fluorination of arylstannanes aryl boronic acids and aryl boronic esters without azeotropic drying [O] . Salla Orvokki Lahdenpohja, Noora Annika Rajala, Johan Rajander, 2019

机译：快速高效的铜介导的18F氟化芳基斯坦酮芳基硼酸和芳基硼酸酯无需共沸干燥
7. Alginate-Polymer-Caged, C-18-Functionalized Magnetic Titanate Nanotubes for Fast and Efficient Extraction of Phthalate Esters from Water Samples with Complex Matrix [O] . Niu Hongyun, Zhang Shengxiao, Zhang Xiaole, 2010

机译：海藻酸酯-聚合物笼装，C-18功能化磁性钛酸酯纳米管，可从复杂基质的水样品中快速高效提取邻苯二甲酸酯。
8. Results of Log Pow Measurement with Propylidynetrimethanol, Propoxylated, Esters with Fatty Acids, C16-18 and C18-22-usatd. [R] . 2014

机译：用丙炔基三甲醇，丙氧基化，脂肪酸酯，C16-18和C18-22-usatd测量Log pow的结果。

Fast and Efficient ~(18)F-Labeling by [~(18)F]Fluorophenylazocarboxylic Esters

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