Unexpected Michael Additions on the Way to 2.3,8.9-Dibenzanthanthrenes with Interesting Structural Properties

Reus Christian; Lechner Marc P.; Schulze Matthias; Lungerich Dominik; Diner Colin; Gruber Marco; Stryker Jeffrey M.; Hampel Frank; Jux Norbert; Tykwinski Rik R.

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Unexpected Michael Additions on the Way to 2.3,8.9-Dibenzanthanthrenes with Interesting Structural Properties

机译：具有意想不到的结构特性的2.3,8.9-二苯并蒽蒽的意外Michael加成

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The synthesis and properties of a new polycyclic aromatic hydrocarbon containing eight annulated rings and based on the anthanthrene core is described. An unexpected, nucleophile-dependent Michael addition to a dibenzanthanthrene-1,7-dione is found, giving a product with three triisopropylsilylacetylene units and a remarkable solid-state structure (as determined by X-ray crystallography).

机译：描述了一种新的包含八环环和基于蒽环的多环芳烃的合成和性能。发现了对苯二氮杂蒽-1，7-二酮的意外的，依赖亲核试剂的迈克尔加成，得到具有三个三异丙基甲硅烷基乙炔单元和显着的固态结构的产物（通过X射线晶体学测定）。

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来源
《Chemistry: A European journal》 |2016年第27期|共5页
作者
Reus Christian; Lechner Marc P.; Schulze Matthias; Lungerich Dominik; Diner Colin; Gruber Marco; Stryker Jeffrey M.; Hampel Frank; Jux Norbert; Tykwinski Rik R.;
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正文语种 eng
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acenediones; acenes; anthanthrene; organic semiconductors; polycyclic aromatic hydrocarbons;

机译：cen烯;并苯;蒽;有机半导体;多环芳烃;

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1. Unexpected Michael Additions on the Way to 2.3,8.9-Dibenzanthanthrenes with Interesting Structural Properties [J] . Reus Christian, Lechner Marc P., Schulze Matthias, Chemistry: A European journal . 2016,第27期

机译：具有意想不到的结构特性的2.3,8.9-二苯并蒽蒽的意外Michael加成
2. Amberlyst-15 catalyzed Michael addition of beta-dicarbonyl compounds to the enones and unexpected ring closure products [J] . Gunduz Hande, Ece Hamdiye, Atsay Armagan, Tetrahedron . 2017,第30期

机译：Amberlyst-15催化的迈克尔向肿块中添加了β-二羰基化合物和意外的环闭合产品
3. Unexpected Synthesis of 2,3,5,6-Tetrahydro-1H-pyrrolo[3,4-c]- pyridine-1,3,6-triones by a Double Michael Addition/CS_2 Extrusion/Double Cyclization Sequence [J] . Giacomo Mari, Lucia De Crescentini, Gianfranco Favi, European journal of organic chemistry . 2017,第42期

机译：2,3,5,6-四氢-1H-吡咯的意外合成[3,4-C] - 吡啶-1,3,6-三酮通过双迈克尔添加/ Cs_2挤出/双环化序列
4. Effect of Zn Addition On Structural, Magnetic Properties, Antistructural Modeling Of Co_(1-x)Zn_xFe204 Nano ferrite [C] . S. Raghuvanshi, S. N. Kane, T. R. Tatarchuk, International Conference on Condensed Matter and Applied Physics . 2017

机译：Zn添加对结构，磁性，CO_（1-X）Zn_XFE204纳米铁氧体的抗体性建模的影响
5. Microstructural Evolution and Mechanical Properties in Aluninum-Scandium Alloys With Lithium and Rare Earth Additions. [D] . Krug, Matthew E. 2011

机译：含锂和稀土的铝-合金的微观结构演变和力学性能。
6. Structural analysis of the dual-function thioesterase SAV606 unravels the mechanism of Michael addition of glycine to an αβ-unsaturated thioester [O] . Taichi Chisuga, Akimasa Miyanaga, Fumitaka Kudo, 2017

机译：双功能硫酯酶SAV606的结构分析揭示了甘氨酸向αβ-不饱和硫酯添加迈克尔的机理
7. Bijvoet in solution reveals unexpected stereoselectivity in a Michael addition. [O] . Sun H., dAuvergne E., Reinscheid U., 2011

机译：解决方案中的Bijvoet在迈克尔的添加中显示出意想不到的立体选择性。

Unexpected Michael Additions on the Way to 2.3,8.9-Dibenzanthanthrenes with Interesting Structural Properties

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