One-Step High-Temperature Solvothermal Synthesis of TiO2/Sulfide Nanocomposite Spheres and Their Solar Visible-Light Applications

Shangjun Ding; Xin Yin; Xujie Lu

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One-Step High-Temperature Solvothermal Synthesis of TiO2/Sulfide Nanocomposite Spheres and Their Solar Visible-Light Applications

机译：一步法高温溶剂热合成TiO2 /硫化物纳米复合球及其在太阳可见光中的应用

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A one-step high-temperature hydrated-sulfate assisted solvothermal method has been developed to synthesize TiO2/sulfide nanocomposite spheres. Different hybrid spheres of TiO2/CdS, TiO2/Cu2S, TiO2/FeS, TiO2/Co9S8, and TiO2/ZnS were readily prepared by exploiting different hydrated sulfate. The hydrated sulfate has been proved to play multifunctional roles during the synthetic process, such as spherical template, water supplier, and composition controller. Nanocrystal CdS can be reduced from CdSO4 at a high solvothermal temperatureof 350 °C, and the TiO2/CdS nanocomposite spheres prepared by this method exhibit superior visible-light-driven photocatalyticefficiency because of its effective heterointerface and high crystallinity.

机译：已经开发出了一步式高温水合硫酸盐辅助溶剂热法来合成TiO2 /硫化物纳米复合球。利用不同的水合硫酸盐可以很容易地制备出不同的TiO2 / CdS，TiO2 / Cu2S，TiO2 / FeS，TiO2 / Co9S8和TiO2 / ZnS杂化球。事实证明，水合硫酸盐在合成过程中起着多功能作用，例如球形模板，水供应商和成分控制剂。可以在350℃的高溶剂热温度下将CdSO4还原成纳米晶CdS，并且该方法制备的TiO2 / CdS纳米复合球由于其有效的异质界面和高结晶度而具有优异的可见光驱动光催化效率。

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《ACS applied materials & interfaces》 |2012年第1期|共6页
作者
Shangjun Ding; Xin Yin; Xujie Lu;
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titanium dioxide; nanocomposite; solvothermal method; visible-light photocatalysis; hydrated sulfate;

机译：二氧化钛;纳米复合材料;溶剂热法;可见光催化;水合硫酸盐;

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1. One-Step High-Temperature Solvothermal Synthesis of TiO2/Sulfide Nanocomposite Spheres and Their Solar Visible-Light Applications [J] . Shangjun Ding, Xin Yin, Xujie Lu ACS applied materials & interfaces . 2012,第1期

机译：一步法高温溶剂热合成TiO2 /硫化物纳米复合球及其在太阳可见光中的应用
2. One-step synthesis of CuO/TiO2 nanocomposite by atmospheric microplasma electrochemistry - Its application as photoanode in dye-sensitized solar cell [J] . Mahmoudabadi Zohreh Dehghani, Eslami Esmaeil Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics . 2019,第期

机译：大气显微电化学CuO / TiO2纳米复合材料的一步合成 - 其在染料敏化太阳能电池中的光电阳极应用
3. One-Step Synthesis of TiO2/Graphene Nanocomposites by Laser Pyrolysis with Well-Controlled Properties and Application in Perovskite Solar Cells [J] . Rapha?lle Belchi, Aurélie Habert, Eddy Foy, ACS Omega . 2019,第7期

机译：用良好控制性能激光热解的TiO2 /石墨烯纳米复合物的一步合成及在钙钛矿太阳能电池中的应用
4. INTERFACE BONDING EFFECT BETWEEN TERNARY SULFIDE SOLID SOLUTION AND TIO2NTS COMPOSITE BY SOLVOTHERMAL SYNTHESIS [C] . Zhongping Yao, Fangzhou Jia, Zhenxing Yu ACS National Meeting Exhibition . 2015

机译：通过溶剂质合成三元硫化物固体溶液与TiO2NTS复合材料的界面粘合效应
5. Solvothermal Process Assisted Sensitization of 1D Anodized TiO2 Nanotubes with 0D Cadmium Chalcogenides (CdTe, CdS) for Efficient Solar to Clean Energy Generation. [D] . Sarker, Swagotom. 2014

机译：溶剂热过程辅助使用0D硫属硫化物（CdTe，CdS）的1D阳极氧化TiO2纳米管的增感，以有效地清洁太阳能。
6. One-Step Synthesis of TiO2/Graphene Nanocompositesby Laser Pyrolysis with Well-Controlled Properties and Applicationin Perovskite Solar Cells [O] . Raphaëlle Belchi, Aurélie Habert, Eddy Foy, 2019

机译：一步法合成TiO2 /石墨烯纳米复合材料性能良好的激光热解法制备及应用在钙钛矿太阳能电池中
7. One-Step Synthesis of TiO2/Graphene Nanocomposites by Laser Pyrolysis with Well-Controlled Properties and Application in Perovskite Solar Cells [O] . -1

机译：用良好控制性能激光热解的TiO2 /石墨烯纳米复合物的一步合成及在钙钛矿太阳能电池中的应用

One-Step High-Temperature Solvothermal Synthesis of TiO2/Sulfide Nanocomposite Spheres and Their Solar Visible-Light Applications

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