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One-pot synthesis of AuPt alloyed nanoparticles by intense x-ray irradiation

机译:强烈的X射线一锅法合成AuPt合金纳米颗粒

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摘要

We synthesized AuPt alloyed nanoparticles in colloidal solution by a one-pot procedure based on synchrotron x-ray irradiation in the presence of PEG (polyethylene glycol). The exclusive presence of alloyed nanoparticles with fcc structure was confirmed by several different experiments including UV-vis spectroscopy, x-ray diffraction (XRD) and transmission electron microscopy (TEM). The composition of the AuPt alloyed nanoparticles can be varied in a continuous fashion by simply varying the feed ratios of Au and Pt precursors. The nanoparticles exhibited colloidal stability and biocompatibility, important for potential applications.
机译:我们基于在PEG(聚乙二醇)存在下的同步加速器X射线辐射,通过一锅法在胶体溶液中合成了AuPt合金纳米颗粒。通过几个不同的实验,包括紫外可见光谱,X射线衍射(XRD)和透射电子显微镜(TEM),证实了具有fcc结构的合金纳米颗粒的唯一存在。通过简单地改变Au和Pt前体的进料比,可以连续地改变AuPt合金纳米颗粒的组成。纳米颗粒表现出胶体稳定性和生物相容性,对于潜在的应用很重要。

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