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Electrodeposition of textured nickel on nickel alloy Hastelloy

机译:在镍合金哈氏合金上电沉积织构化镍

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摘要

We proposed a new method fabricating low-cost and mechanically strong tapes for coated conductors. In this method, Hastelloy (R) tape, which is a strong nickel alloy, is plated with a nickel film. A two-step plating was applied to obtain a textured nickel film. In the first step, a strike bath was used in order to plate a nickel film on Hastelloy surface. In the second step, the film was plated in a low cost watts bath. We controlled various plating conditions such as pH-condition, thickness, and current density in the watts bath to fabricate a textured nickel film. The crystal orientation of the nickel films was characterized by an X-ray diffraction method (XRD) with Cu K alpha radiation. Preferred orientation of the film depends on pH of watts bath, nickel film thickness, and current density. The optimal conditions for obtaining a textured nickel film are pH of 4.5 for the watts bath, current density of 500 A/m(2), and thickness of 92 pm. Finally, we succeeded in obtaining nickel films with 96% c-axis orientation.
机译:我们提出了一种制造低成本和机械强度高的带状导体带的新方法。在这种方法中,将坚固的镍合金Hastelloy(R)胶带镀镍膜。进行两步电镀以获得带纹理的镍膜。在第一步中,使用冲击浴来在镍基合金表面上镀镍膜。在第二步中,将膜镀在低成本瓦特浴中。我们控制了各种电镀条件,例如瓦特浴中的pH条件,厚度和电流密度,以制造带纹理的镍膜。镍膜的晶体取向通过具有Cu Kα辐射的X射线衍射法(XRD)来表征。膜的优选取向取决于瓦特浴的pH,镍膜厚度和电流密度。获得带纹理的镍膜的最佳条件是瓦特浴的pH值为4.5,电流密度为500 A / m(2),厚度为92 pm。最后,我们成功地获得了c轴方向为96%的镍膜。

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