A structural and H-1 NMR relaxometric study on novel layered carboxyalkylaminophosphonate nanocrystals with Gd(III) ions located in the framework

Scafuri Antonio; Vivani Riccardo; Carniato Fabio; Tei Lorenzo; Botta Mauro; Taddei Marco; Costantino Ferdinando

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A structural and H-1 NMR relaxometric study on novel layered carboxyalkylaminophosphonate nanocrystals with Gd(III) ions located in the framework

机译：结构和H-1 NMR弛豫研究新型Gd（III）离子位于框架中的层状羧烷基氨基膦酸酯纳米晶体

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Novel Gd(III) carboxyalkylphosphonate nanocrystals were synthesized under mild hydrothermal conditions. Structural properties and H-1 NMR relaxometric behaviour in aqueous solution as a function of the magnetic field strength were investigated, aiming to evaluate the local chemical environment of the paramagnetic centres and their interaction and affinity with water molecules.

机译：在温和的水热条件下合成了新型的Gd（III）羧基烷基膦酸酯纳米晶体。研究了水溶液的结构性质和H-1 NMR弛豫行为随磁场强度的变化，旨在评估顺磁中心的局部化学环境及其与水分子的相互作用和亲和力。

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《Dalton transactions: An international journal of inorganic chemistry》 |2015年第44期|共4页
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Scafuri Antonio; Vivani Riccardo; Carniato Fabio; Tei Lorenzo; Botta Mauro; Taddei Marco; Costantino Ferdinando;
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1. A structural and H-1 NMR relaxometric study on novel layered carboxyalkylaminophosphonate nanocrystals with Gd(III) ions located in the framework [J] . Scafuri Antonio, Vivani Riccardo, Carniato Fabio, Dalton transactions: An international journal of inorganic chemistry . 2015,第44期

机译：结构和H-1 NMR弛豫研究新型Gd（III）离子位于框架中的层状羧烷基氨基膦酸酯纳米晶体
2. H-1 and O-17 NMR relaxometric study in aqueous solution of Gd(III) complexes of EGTA-like derivatives bearing methylenephosphonic groups [J] . Tei L, Botta M, Lovazzano C, Magnetic Resonance in Chemistry: MRC . 2008,第Suppla期

机译：带有亚甲基膦酸酯基团的EGTA类衍生物的Gd（III）配合物在水溶液中的H-1和O-17 NMR弛豫研究
3. RELAXOMETRIC, STRUCTURAL, AND DYNAMIC NMR STUDIES OF DOTA-LIKE LN(III) COMPLEXES (LN=LA, GD, HO, YB) CONTAINING A P-NITROPHENYL SUBSTITUENT [J] . Aime S., Ermondi G., Terreno E., Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics . 1996,第10期

机译：含对亚硝基苯取代基的类似Dota的LN（III）配合物（LN = LA，GD，HO，YB）的重共轴，结构和动态NMR研究
4. DYNAMIC LIGHT SCATTERING AND RELAXOMETRIC STUDIES OF WATER-SOLUBLE Gd@C_+(60) DERIVATIVES AS pH-RESPONSIVE MRI CONTRAST AGENTS [C] . Balaji Sitharaman, Lon J. Wilson, Robert D. Bolskar, Electrochemical Society Annual Meeting . 2005

机译：作为pH响应MRI造影剂的水溶性GD @ C _ +（60）衍生物的动态光散射和放松研究
5. 1- and 2-dimensional proton, carbon-13, and platinum-195 NMR studies of platinum(EDTA) dichloride in heavy water solution and structural characterization of several iron(III) tris(2-pyridylmethyl)amine complexes. [D] . Mullaney, Matthew. 1996

机译：重水溶液中二氯化铂（EDTA）的一维和二维质子，碳13和铂-195 NMR研究以及几种铁（III）三（2-吡啶基甲基）胺络合物的结构表征。
6. Structural determinants of fluoride and formate binding to hemoglobin and myoglobin: crystallographic and 1H-NMR relaxometric study. [O] . S Aime, M Fasano, S Paoletti, 1996

机译：氟化物和甲酸盐与血红蛋白和肌红蛋白结合的结构决定因素：晶体学和1 H-NMR弛豫研究。
7. H5EPTPACH2OH: Synthesis, relaxometric characterization and H-1 NMR studies of the solution dynamics of its Ln(III) complexes [O] . Martins, Ja., André, Jp., Pereira, Ga., 2007

机译：H5EPTPACH2OH：Ln（III）配合物的溶液动力学的合成，弛豫特征和H-1 NMR研究

A structural and H-1 NMR relaxometric study on novel layered carboxyalkylaminophosphonate nanocrystals with Gd(III) ions located in the framework

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