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首页> 外文期刊>Dalton transactions: An international journal of inorganic chemistry >Efficient microwave assisted synthesis of metal-organic framework UiO-66: optimization and scale up
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Efficient microwave assisted synthesis of metal-organic framework UiO-66: optimization and scale up

机译：高效微波辅助合成金属有机骨架UiO-66：优化和放大

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摘要

A highly efficient and scalable microwave assisted synthesis of zirconium-based metal-organic framework UiO-66 was developed. In order to identify the best conditions for optimizing the process, a wide range of parameters was investigated. The efficiency of the process was evaluated with the aid of four quantitative indicators. The properties of the materials prepared by microwave irradiation were compared with those synthesized by conventional heating, and no significant effects on morphology, crystal size, or defects were found from the use of microwave assisted heating. Scale up was performed maintaining the high efficiency of the process.
机译：开发了一种高效，可扩展的微波辅助合成锆基金属有机骨架UiO-66。为了确定优化工艺的最佳条件，对各种参数进行了研究。借助四个定量指标评估了流程的效率。将通过微波辐射制备的材料的性能与通过常规加热合成的材料的性能进行了比较，并且通过使用微波辅助加热未发现对形态，晶体尺寸或缺陷有显着影响。进行放大以保持过程的高效率。

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