Improvement in alkoxide anionic initiation technique by using a colorimetric titration

Compos D; Delaite C; Hurtrez G; Dumas P

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Improvement in alkoxide anionic initiation technique by using a colorimetric titration

机译：通过比色滴定法改进醇盐阴离子引发技术

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We developed a colorimetric method to follow and to control the complete transformation of an alcohol into an alkoxide. It was first tested on a small molecule and then extended to a macroinitiator. It allows us to obtain a final product without residual prepolymer and without side initiation due to an excess of carbanion. (c) 2005 Wiley Periodicals, Inc.

机译：我们开发了一种比色法，以遵循并控制醇向醇盐的完全转化。首先在小分子上进行测试，然后扩展到大分子引发剂上。它允许我们获得最终产品，而没有残留的预聚物，也没有由于过量的碳负离子而引起的侧链引发。（c）2005年Wiley Periodicals，Inc.

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《Journal of Applied Polymer Science》 |2005年第3期|共5页
作者
Compos D; Delaite C; Hurtrez G; Dumas P;
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正文语种 eng
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anionic polymerization; colorimetry; initiatiors; living polymerization; titration; OXIDE) DIBLOCK COPOLYMERS;

机译：阴离子聚合;比色法;引发剂;活性聚合;滴定;氧化物）二嵌段共聚物;

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1. Improvement in alkoxide anionic initiation technique by using a colorimetric titration [J] . Compos D, Delaite C, Hurtrez G, Journal of Applied Polymer Science . 2005,第3期

机译：通过比色滴定法改进醇盐阴离子引发技术
2. Initiation of styrene retarded anionic polymerization using the combination of lithium alkoxides with organometallic compounds [J] . Menoret S., Fontanille M., Deffieux A., Macromolecules . 2002,第12期

机译：结合使用醇锂和有机金属化合物引发苯乙烯阻滞阴离子聚合
3. Alkoxide initiation of anionic polymerization of masked disilenes to polysilanes [J] . Sanji T., Sakurai H., Kawabata K. Journal of Organometallic Chemistry . 2000,第1a2期

机译：掩蔽二烯类化合物向聚硅烷的阴离子聚合的醇盐引发
4. Activation Mechanisms of Trialkylaluminum in Alkali Metal Alkoxides or Tetraalkylammonium Salts / Propylene Oxide Controlled Anionic Polymerization [C] . Stephane Carlotti, Cyrille Billouard, Emilie Gautriaud, World Polymer Congress . 2005

机译：碱金属醇醇铝中三烷基铝的活化机制或四烷基铵盐/环氧丙烷控制的阴离子聚合
5. Anionic synthesis of highly isotactic polystyrene in the presence of lithium hydroxides or lithium alkoxides, and, Controlled "living" emulsion polymerization of methyl methacrylate by atom transfer radical polymerization. [D] . Makino, Takayuki. 1997

机译：在氢氧化锂或烷氧基锂的存在下阴离子合成高度全同立构的聚苯乙烯，以及通过原子转移自由基聚合进行甲基丙烯酸甲酯的受控“活”乳液聚合。
6. An exploratory trial of insulin initiation and titration among patients with type 2 diabetes in the primary care setting with retrospective continuous glucose monitoring as an adjunct: INITIATION study protocol [O] . Irene D Blackberry, John S Furler, Louise E Ginnivan, 2014

机译：在初级保健机构中对2型糖尿病患者进行胰岛素启动和滴定的一项探索性试验并辅以回顾性连续血糖监测：INITIATION研究方案
7. A Computational Study of Anionic Alkoxide-Allene and Amide-Allene Cyclizations [O] . Florimond Cumine, Allan Young, Hans-Ulrich Reissig, 2017

机译：阴离子醇盐 - 苯烯和酰胺苯甲酸苯甲酸烯的计算研究
8. Improved Colorimetric Methods and Field Test Kits for Analyzing Anionic Surfactants in Water and Wastewater [R] . Wang, L. K. 1973

机译：改进的比色法和现场试验试剂盒分析水和废水中的阴离子表面活性剂

Improvement in alkoxide anionic initiation technique by using a colorimetric titration

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