Synthesis and characterization of amphiphilic polymer networks based on acrylated poly(epsilon-caprolactone) and N-vinylpyrrolidone

Liao LQ; Zhang C; Gong SQ

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Synthesis and characterization of amphiphilic polymer networks based on acrylated poly(epsilon-caprolactone) and N-vinylpyrrolidone

机译：基于丙烯酸化聚ε-己内酯和N-乙烯基吡咯烷酮的两亲聚合物网络的合成与表征

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New amphiphilic polymer networks were synthesized by the free-radical copolymerization of alpha omega-diacryl polycaprolactone (DAPCL) and N-vinylpyrrolidone (NVP), which was initiated by 0.5% azobisisobutyronitrile at 70 degrees C. The chemical structures of the networks were characterized by proton nuclear magnetic resonance spectrometry. The NVP/DAPCL feed ratio played an important role in the crosslinking process. The synthesized amphiphilic polymer networks exhibited controlled swelling properties in water and organic solvents (ethanol, acetones, and toluene). A porous structure was observed for the amphiphilic polymer networks under a scanning electron microscope. (C) 2007 Wiley Periodicals, Inc.

机译：通过αω-二丙烯酸聚己内酯（DAPCL）和N-乙烯基吡咯烷酮（NVP）的自由基共聚反应合成了新的两亲聚合物网络，该网络由70％的0.5％偶氮二异丁腈引发。质子核磁共振光谱法。 NVP / DAPCL进料比在交联过程中起重要作用。合成的两亲聚合物网络在水和有机溶剂（乙醇，丙酮和甲苯）中具有受控的溶胀特性。在扫描电子显微镜下观察到两亲性聚合物网络的多孔结构。（C）2007 Wiley期刊公司

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《Journal of Applied Polymer Science》 |2007年第5期|共5页
作者
Liao LQ; Zhang C; Gong SQ;
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正文语种 eng
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copolymerization; amphiphilic; networks; SWELLING BEHAVIOR; MACROMONOMERS; POLYLACTIDES; COPOLYMERS; STRATEGIES; DELIVERY; RELEASE; INSULIN;

机译：共聚;两亲;网络;溶胀行为;宏观单体;聚乳酸;共聚物;策略;交付;释放;胰岛素;

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1. Synthesis and characterization of amphiphilic polymer networks based on acrylated poly(epsilon-caprolactone) and N-vinylpyrrolidone [J] . Liao LQ, Zhang C, Gong SQ Journal of Applied Polymer Science . 2007,第5期

机译：基于丙烯酸化聚ε-己内酯和N-乙烯基吡咯烷酮的两亲聚合物网络的合成与表征
2. Synthesis of poly(epsilon-caprolactone)-block-poly(n-butyl acrylate) by combining ring-opening polymerization and atom transfer radical polymerization with Ti[OCH2CCl3](4) as difunctional initiator: I. Kinetic study of Ti[OCH2CCl3](4) initiated ring-opening polymerization of epsilon-caprolactone [J] . Li PC, Zerroukhi A, Chen JD, Polymer: The International Journal for the Science and Technology of Polymers . 2009,第5期

机译：Ti [OCH2CCl3]（4）为双官能团引发剂的开环聚合和原子转移自由基聚合的合成聚（ε-己内酯）-嵌段-聚丙烯酸正丁酯：I. Ti [OCH2CCl3]的动力学研究（4）引发ε-己内酯的开环聚合
3. Synthesis and Characterization of Amphiphilic Poly(N-vinyl pyrrolidone)-b-poly(epsilon-caprolactone) Copolymers by a Combination of Cobalt-Mediated Radical Polymerization and Ring-Opening Polymerization [J] . Jeon HJ, You YC, Youk JH Journal of Polymer Science, Part A. Polymer Chemistry . 2009,第12期

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4. Synthesis and Permeabilities of Novel Amphiphilic Polymer Conetworks Based on Poly(N-vinylpyrrolidone) and Polydimethylsiloxane [C] . WANG Dan-dan, LI Xiao-lei, HE Chun-ju, 2010 International Forum on Biomedical Textile Materials(2010国际纺织生物医用论坛） . 2010

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Synthesis and characterization of amphiphilic polymer networks based on acrylated poly(epsilon-caprolactone) and N-vinylpyrrolidone

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