Synthesis of N-beta-Aminoethyl-gamma-aminopropyl Polydimethyl-co-polydiphenylsiloxane and Its Film Morphology and Orientation

Li MT; An QF; Huang LX; Yang G; Wang QJ

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Synthesis of N-beta-Aminoethyl-gamma-aminopropyl Polydimethyl-co-polydiphenylsiloxane and Its Film Morphology and Orientation

机译：N-β-氨基乙基-γ-氨基丙基聚二甲基-co-聚二苯基硅氧烷的合成及其膜形貌和取向

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A fabric softner, N-beta-aminoethyl-gamma-aminopropyl polydimethyl-co-polydiphenylsiloxane (PASO), was synthesized by the polymerization of octamethyl cyclotetrasiloxane with an amino-functional silane and dimethyldiphenysilane. The chemical structure of the synthesized polysiloxane was characterized by Fourier transform infrared and H-1-NMR spectra. The morphology, composition, and hydrophobic properties of the PASO film were investigated by X-ray photoelectron spectroscopy, atomic force microscopy, contact angle measurement, and other measurements. The experimental results indicate that on the silicon wafer surface, PASO formed a hydrophobic, nonhomogeneous structural film. In addition, the atomic force microscopy results show that the PASO film deposited on the silicon wafer seemed to be slightly rougher than the film of the control, the N-beta-aminoethyl-gamma-aminopropyl polydimethylsiloxane. As a result, an orientation model of PASO is proposed on the basis of the characterization of the PASO film properties. (C) 2008 Wiley Periodicals, Inc. J Appl Polym Sci 111: 2715-2719, 2009

机译：通过八甲基环四硅氧烷与氨基官能硅烷和二甲基二苯基硅烷的聚合反应，合成了一种织物柔软的N-β-氨基乙基-γ-氨基丙基聚二甲基-共聚二苯基硅氧烷（PASO）。合成的聚硅氧烷的化学结构通过傅立叶变换红外光谱和H-1-NMR光谱表征。通过X射线光电子能谱，原子力显微镜，接触角测量和其他测量研究了PASO膜的形态，组成和疏水性。实验结果表明，PASO在硅晶片表面上形成了疏水的非均质结构膜。另外，原子力显微镜结果表明，沉积在硅晶片上的PASO膜似乎比对照N-β-氨基乙基-γ-氨基丙基聚二甲基硅氧烷的膜稍粗糙。结果，基于PASO膜性质的表征，提出了PASO的取向模型。（C）2008 Wiley Periodicals，Inc. J Appl Polym Sci 111：2715-2719，2009

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来源
《Journal of Applied Polymer Science》 |2009年第6期|共5页
作者
Li MT; An QF; Huang LX; Yang G; Wang QJ;
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正文语种 eng
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atomic force microscopy (AFM); films; morphology; orientation; polysiloxanes; FUNCTIONAL POLYSILOXANE; SOFTENERS; POLYMERS;

机译：原子力显微镜（AFM）;膜;形貌;取向;聚硅氧烷;功能性聚硅氧烷;软化剂;聚合物;

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1. Synthesis of N-beta-Aminoethyl-gamma-aminopropyl Polydimethyl-co-polydiphenylsiloxane and Its Film Morphology and Orientation [J] . Li MT, An QF, Huang LX, Journal of Applied Polymer Science . 2009,第6期

机译：N-β-氨基乙基-γ-氨基丙基聚二甲基-co-聚二苯基硅氧烷的合成及其膜形貌和取向
2. Influence of substrate orientation on the morphology and orientation of LaNiO3 thin films. [J] . Pocuca M, Brankovic Z, Brankovic G Journal of Microscopy . 2008,第3期

机译：衬底取向对LaNiO3薄膜形态和取向的影响。
3. The annealing temperature and films thickness effect on the surface morphology, preferential orientation and dielectric property of NiO films [J] . Yang Pan, Li Lingxia, Yu Shihui, Applied Surface Science . 2019,第Nova1期

机译：退火温度和膜厚对NiO膜表面形貌，择优取向和介电性能的影响
4. Growth orientation and surface morphology of CeO_2 films for high-Jc YBCO films on biaxialh -textured Ni tape by PLD [C] . Huaran Liu, Linfei Liu, Xiaokun Song, International conference on thin film physics and applications . 2011

机译：PLD法在双轴织构Ni带上制备高Jc YBCO薄膜的CeO_2薄膜的生长方向和表面形貌
5. Effect of orientation on the physicochemical and morphological changes in absorbing polylactide films. [D] . Burg, Karen Jane Leadbetter. 1996

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6. Direct Synthesis of Anatase Films with ~100 (001) Facets and 001 Preferred Orientation [O] . Andrew S. Ichimura, Brianne Mack, Shirin M. Usmani, -1

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7. Pulsed Laser Deposition of Zinc Sulfide Thin Films on Silicon: The influence of substrate orientation and preparation on thin film morphology and texture [O] . Heimdal Carl Philip J 2014

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Synthesis of N-beta-Aminoethyl-gamma-aminopropyl Polydimethyl-co-polydiphenylsiloxane and Its Film Morphology and Orientation

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