Investigation of Factors Affecting Synthesis of Polyvinyl Butyral by Taguchi Method

Hajian M; Koohmareh GA; Rastgoo M

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Investigation of Factors Affecting Synthesis of Polyvinyl Butyral by Taguchi Method

机译：田口法合成聚乙烯醇缩丁醛的影响因素研究

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Polyvinyl butyral (PVB) was prepared by condensation reaction of butyral with polyvinyl alcohol (PVA) in aqueous phase containing an acid as a catalyst and an emulsifying agent. Properties of the polymer were a function of the relative amounts of the three randomly distributed units of acetal, acetate and vinyl alcohol groups, and the molecular weight. In this work, some effective factors in synthesis of PVB have been investigated by Taguchi method. The percent of the acetalization has been determined according to the ASTM D1396, and the polymer was characterized by IR, TG, and DTG techniques.

机译：通过使丁缩醛与聚乙烯醇（PVA）在含有酸作为催化剂和乳化剂的水相中缩合反应来制备聚乙烯醇缩丁醛（PVB）。聚合物的性质是乙醛，乙酸酯和乙烯醇基团的三个随机分布单元的相对量以及分子量的函数。在这项工作中，通过Taguchi方法研究了一些合成PVB的有效因素。缩醛化的百分比已根据ASTM D1396确定，并且聚合物通过IR，TG和DTG技术进行了表征。

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来源
《Journal of Applied Polymer Science》 |2010年第6期|共6页
作者
Hajian M; Koohmareh GA; Rastgoo M;
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正文语种 eng
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modification; polycondensation; synthesis; thermogravimetric analysis (TGA);

机译：改性;缩聚;合成;热重分析（TGA）;

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1. Investigation of Factors Affecting Synthesis of Polyvinyl Butyral by Taguchi Method [J] . Hajian M, Koohmareh GA, Rastgoo M Journal of Applied Polymer Science . 2010,第6期

机译：田口法合成聚乙烯醇缩丁醛的影响因素研究
2. Constitutive Investigation on Viscoelasticity of PolyVinyl Butyral: Experiments Based on Dynamic Mechanical Analysis Method [J] . BohanLiu, JunXu, YibingLi Advances in materials science and engineering . 2014,第1期

机译：聚乙烯醇缩丁醛粘弹性的本构研究：基于动态力学分析方法的实验
3. Synthesis of ZSM-5 with intracrystal or intercrystal mesopores by polyvinyl butyral templating method [J] . Zhu HB, Liu ZC, Kong DJ, Journal of Colloid and Interface Science . 2009,第2期

机译：聚乙烯醇缩丁醛模板法合成具有晶内或晶间中孔的ZSM-5
4. The Weight of Influence of Factors on Microtrigeneration Systems (mCCHP) Using Taguchi Methods [C] . NELU CAZACU, NICOLAE BADEA Non-Linear systems and wavelet analysis . 2010

机译：Taguchi方法的因素对微三代系统（mCCHP）的影响权重
5. NEW SYNTHETIC METHODS IN ORGANIC CHEMISTRY: PART I. THE SYNTHESIS AND REACTIVITY OF STERICALLY HINDERED NITRIMINES--SYNTHESIS OF IMINES. PART II. INVESTIGATIONS INTO THE SYNTHESIS AND COUPLING REACTIONS OF 1,3-DITHIOLE ANALOGS. [D] . RUSSO, JOSEPH MICHAEL. 1986

机译：有机化学的新合成方法：第一部分：空间受限的亚硝酸盐的合成和反应性—氨基酸的合成。第二部分1,3-二噻吩类似物的合成和偶联反应的研究。
6. Application of Taguchi Method to Investigate the Effects of Process Factors on the Production of Industrial Piroxicam Polymorphs and Optimization of Dissolution Rate of Powder [O] . Alen Shahbazian, Asghar Davood, Alireza Dabirsiaghi 2016

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7. Constitutive Investigation on Viscoelasticity of PolyVinyl Butyral: Experiments Based on Dynamic Mechanical Analysis Method [O] . Bohan Liu, Jun Xu, Yibing Li 2014

机译：基于动态机械分析法的聚乙烯醇抑制性粘弹性的组成型研究

Investigation of Factors Affecting Synthesis of Polyvinyl Butyral by Taguchi Method

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