Dynamic Cure Kinetics of Epoxy-Novolac Compounds as Studied by Differential Scanning Calorimetry

Yang SS; Hsieh TH; Bi HT; Ho KS; Ho TH; Chen HR; Ye SH; Chang YC

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Dynamic Cure Kinetics of Epoxy-Novolac Compounds as Studied by Differential Scanning Calorimetry

机译：差示扫描量热法研究环氧-酚醛清漆化合物的动态固化动力学

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The cure kinetics of epoxy-novolac compounds were Studied by means of differential scanning calorimetry with a dynamic approach. On the basis of a modified version of our previously reported kinetic model, a procedure aiming at the phenomenological description of the cure kinetics was developed. The reactions were found to be autocatalytic in nature for both commercial epoxy-novolac molding compounds and silica-free imidazole-cured epoxy-novolac systems. The weak extent of autocatalysis in the epoxy-novolac molding compounds was likely due to their high content of silica fillers.

机译：通过差示扫描量热法和动态方法研究了环氧酚醛清漆化合物的固化动力学。在我们先前报道的动力学模型的改进版本的基础上，针对固化动力学的现象学描述开发了一种方法。发现该反应本质上对于市售的环氧-酚醛模塑化合物和无二氧化硅的咪唑固化的环氧-酚醛体系都是自动催化的。环氧酚醛型模塑料中的自催化程度较弱，可能是由于其二氧化硅填料含量高。

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《Journal of Applied Polymer Science》 |2009年第4期|共5页
作者
Yang SS; Hsieh TH; Bi HT; Ho KS; Ho TH; Chen HR; Ye SH; Chang YC;
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正文语种 eng
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curing of polymers; differential scanning calorimetry (DSC); thermosets;

机译：聚合物固化;差示扫描量热法（DSC）;热固性;

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1. Dynamic Cure Kinetics of Epoxy-Novolac Compounds as Studied by Differential Scanning Calorimetry [J] . Yang SS, Hsieh TH, Bi HT, Journal of Applied Polymer Science . 2009,第4期

机译：差示扫描量热法研究环氧-酚醛清漆化合物的动态固化动力学
2. MECHANISM AND KINETICS OF EPOXY-AMINE CURE STUDIED BY DIFFERENTIAL SCANNING CALORIMETRY [J] . Vyazovkin S., Sbirrazzuoli N. Macromolecules . 1996,第6期

机译：差示扫描量热法研究环氧-胺固化的机理和动力学
3. A study on the curing kinetics of epoxy molding compounds with various latent catalysts using differential scanning calorimetry [J] . Lee Da Eun, Kim Hyun Woo, Kong Byung-Seon, Journal of Applied Polymer Science . 2017,第35a36期

机译：用差示扫描量热法与各种潜催化剂的环氧成型化合物固化动力学研究
4. Characterization of Curing Behavior of Phenolic Resins by Differential Scanning Calorimetry: Model-Free Kinetics Compared to Conventional Kinetics [C] . Guangbo He, Bernard Riedl Proceedings of the 31st annual conference of the North American Thermal Analysis Society(NATAS) . 2003

机译：差示扫描量热法表征酚醛树脂的固化行为：与常规动力学相比，无模型动力学
5. Cure Kinetics of Benzoxazine/Cycloaliphatic Epoxy Resin by Differential Scanning Calorimetry. [D] . Gouni, Sreeja Reddy. 2018

机译：差示扫描量热法测定苯并恶嗪/脂环族环氧树脂的固化动力学。
6. Kinetic Analysis of the Curing of a Partially Biobased Epoxy Resin Using Dynamic Differential Scanning Calorimetry [O] . Diego Lascano, Luis Quiles-Carrillo, Rafael Balart, 2019

机译：动态差示扫描量热法对部分生物基环氧树脂固化的动力学分析
7. Cooperativity and Kinetics of Phase Transitions in Nanopore-Confined Bilayers Studied by Differential Scanning Calorimetry [O] . Alaouie, Ali M., Smirnov, Alex I. 2005

机译：差示扫描量热法研究纳米孔受限双层膜的相变协同性和动力学
8. The Kinetics of Polymer Cure by Differential Scanning Calorimetry. Volume I. [R] . Adams, W. W., Goldfarb, I. J. 1982

机译：差示扫描量热法测定聚合物的固化动力学。第一卷

Dynamic Cure Kinetics of Epoxy-Novolac Compounds as Studied by Differential Scanning Calorimetry

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