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Characterization of solvent-spun polyester nanofibers

机译:溶剂纺聚酯纳米纤维的表征

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摘要

The aim of this study was to examine the properties of polyester nanofibers produced by the electrospinning method. Solvent-spun nanofibers with different concentrations of poly(ethylene terephthalate) (13, 16, and 20 wt %) were produced. The morphology and surface energy of the fibers were analyzed by scanning electron microscopy and contact angle measurements. Tensile testing, dynamic mechanical analysis, and differential scanning calorimetry were carried out to characterize the thermal and mechanical properties. X-ray diffraction and attenuated total reflection Fourier transform infrared spectroscopy tests were performed to analyze the microstructural properties. The results show that a nanoweb of the 16 wt % solution had better mechanical and thermal behaviors because of the increased molecular orientation in the amorphous structure and the narrower fiber diameter distribution in the web.
机译:这项研究的目的是检查通过静电纺丝法生产的聚酯纳米纤维的性能。制备了具有不同浓度的聚对苯二甲酸乙二酯(13、16和20 wt%)的溶剂纺丝纳米纤维。通过扫描电子显微镜和接触角测量来分析纤维的形态和表面能。进行拉伸测试,动态力学分析和差示扫描量热法以表征热和机械性能。进行了X射线衍射和衰减全反射傅立叶变换红外光谱测试,以分析其显微结构。结果表明,由于无定形结构中分子取向的增加和纤网中纤维直径的分布较窄,所以16 wt%溶液的纳米纤网具有更好的机械和热行为。

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