Preparation mechanism of (Bi_2O_3)_(0.75)(Dy_2O_3)_(0.25) nano-crystalline solid electrolyte

RongLi; QiangZhen; Michel Drache

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Preparation mechanism of (Bi_2O_3)_(0.75)(Dy_2O_3)_(0.25) nano-crystalline solid electrolyte

机译：（Bi_2O_3）_（0.75）（Dy_2O_3）_（0.25）纳米晶固体电解质的制备机理

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(Bi_2O_3)_(0.75)(Dy_2O_3)_(0.25) nanopowder was prepared by reverse chemical titration co-precipitation method. The reaction mechanism during the precipitation process was discussed by thermodynamic analysis. Thermal decomposition behavior of the precursor was investigated using X-ray diffractometry and TG-MS analysis. The precursor was calcined at 500 °C for 3 h to obtain (Bi_2O_3)_(0.75)(Dy_2O_3)_(0.25) nanopowder. Using the nanopowder, pellets with relative density higher than 94% were obtained at 700 °C for 2 h by pressureless sintering, and the grains remained at the nano-scale with size of 72 nm.

机译：通过反向化学滴定共沉淀法制备了（Bi_2O_3）_（0.75）（Dy_2O_3）_（0.25）纳米粉。通过热力学分析讨论了沉淀过程中的反应机理。使用X射线衍射和TG-MS分析研究了前体的热分解行为。将前体在500℃下煅烧3小时以获得（Bi_2O_3）_（0.75）（Dy_2O_3）_（0.25）纳米粉。使用纳米粉末，通过无压烧结在700℃下2小时获得相对密度高于94％的丸粒，并且晶粒保持在纳米级，尺寸为72nm。

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《Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics》 |2010年第2期|共5页
作者
RongLi; QiangZhen; Michel Drache;
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正文语种 eng
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Reverse chemical titration precipitation; Reaction mechanism; Nano-crystalline ceramic;

机译：反向化学滴定沉淀;反应机理;纳米晶陶瓷;

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1. Preparation mechanism of (Bi_2O_3)_(0.75)(Dy_2O_3)_(0.25) nano-crystalline solid electrolyte [J] . RongLi, QiangZhen, Michel Drache Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics . 2010,第1a2期

机译：（Bi_2O_3）_（0.75）（Dy_2O_3）_（0.25）纳米晶固体电解质的制备机理
2. Characterization of ion transport property and study of solid state battery discharge performance on newly synthesized Ag+ ion conducting quaternary solid electrolyte systems: x[0.75AgI : 0.25AgCl]: (1-x)KI [J] . Agrawal RC, Chandra A, Bhatt A, The European physical journal. Applied physics . 2008,第2期

机译：x [0.75AgI：0.25AgCl]：（1-x）KI在新合成的Ag +离子导电四元固体电解质体系上的离子输运特性表征和固态电池放电性能研究
3. Preparation of perovskite 0.75Pb(Ni1/3Nb2/3)O-3-0.25PbTiO(3) ceramics using semichemical methods and related reaction mechanisms [J] . Cui B, Gao XH, Cheng HL, Chemical Engineering Communications . 2008,第1期

机译：半化学法及相关反应机理制备钙钛矿0.75Pb（Ni1 / 3Nb2 / 3）O-3-0.25PbTiO（3）陶瓷
4. SOLID OXIDE FUEL CELL WITH A La_(0.75)Sr_(0.25)Cr_(0.5)Mn_(0.5)O_(3-δ) ANODE AND AN LSGM ELECTROLYTE [C] . Jen-Hau Wan, J. H. Zhu, John B. Goodenough Proceedings vol.2005-07; International Symposium on Solid Oxide Fuel Cells IX(SOFC-IX) vol 1: Cells, Stacks, and Systems; 20050515-20; Quebec City(CA) . 2005

机译：La_（0.75）Sr_（0.25）Cr_（0.5）Mn_（0.5）O_（3-δ）阳极和LSGM电解质的固体氧化物燃料电池
5. Investigation of (La1-X,Cax)(Ni 0.25Fe0.25Cr0.25Co0.25)O3 for Solid Oxide Fuel Cells Cathode Materials [D] . Gajjala, Sai Ram 2017

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6. A limiting Current Oxygen Sensor Constituted of (CeO2)0.95(Y2O3)0.05 as Solid Electrolyte Layer and (CeO2)0.75(ZrO2)0.25 as Dense Diffusion Barrier Layer [O] . Xiangnan Wang, Tao Liu, Jingkun Yu 2019

机译：由（CeO2）0.95（Y2O3）0.05作为固体电解质层和（CeO2）0.75（ZrO2）0.25作为密集扩散阻挡层组成的极限电流氧传感器
7. Plasma-Sprayed High-Performance (Bi2O3)0.75(Y2O3)0.25 Electrolyte for Intermediate-Temperature Solid Oxide Fuel Cells (IT-SOFCs) [O] . Rui Chen, Shan-Lin Zhang, Chang-Jiu Li, 2021

机译：用于中间温固体氧化物燃料电池的等离子体喷涂的高性能（Bi2O3）0.75（Y2O3）0.25电解质（IT-SOFC）

Preparation mechanism of (Bi_2O_3)_(0.75)(Dy_2O_3)_(0.25) nano-crystalline solid electrolyte

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